Microporous ceramic catalyst carrier and preparation method thereof
A technology of catalyst carrier and microporous ceramics, which is applied in the direction of catalyst carrier, chemical instrument and method, physical/chemical process catalyst, etc., can solve the problem of low universality of catalyst carrier, achieve small density, strong scalability, and The effect of low grain size
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Embodiment 1
[0033] Formula: 78% mass fraction, 300-mesh low-quality bauxite 700°C light-fired material, the composition and mass fraction after light-fired are shown in Table 1.
[0034] Table 1 Composition of bauxite after light burning
[0035] Element
SiO 2 (%)
al 2 o 3 (%)
Fe 2 o 3 (%)
TiO 2 (%)
CaO(%)
MgO(%)
K 2 O(%)
Na 2 O(%)
Ignition loss (%)
content
50.14
44.31
2.84
1.19
0.35
0.22
0.25
0.10
0.60
[0036] Additive, mass fraction 21.1%, purity>99% water-soluble starch.
[0037] Dispersant, mass fraction 0.9% sodium polyacrylate.
[0038] Process:
[0039] (1) Lightly burn low-quality bauxite at 700° C., refine it to 300 mesh by ball milling, add additives with a mass fraction of 21.1% and 0.9% dispersant and mix uniformly to obtain a mixture;
[0040] (2) Add 80% of the mixture to the EIRICH vertical granulator for granulation, add 21% of atomized water, run at 5000rpm / min for 10mi...
Embodiment 2
[0046] Formula: 84% mass fraction, 250 mesh low-quality bauxite 800°C lightly fired material, the composition after lightly fired is shown in Table 2.
[0047] Table 2 Composition of bauxite after light burning
[0048]
[0049] Additives, mass fraction 15%. Purity>99% water-soluble starch.
[0050] Dispersant, mass fraction 1.0% sodium polyacrylate.
[0051] Process:
[0052] (1) Low-quality bauxite is lightly burned at 800°C, ball milled to refine it to 250 mesh, and 15% of additives and 1.0% of dispersant are added to mix uniformly to obtain a mixture;
[0053] (2) Add 84% of the mixture to the EIRICH vertical granulator for granulation, add 18% of atomized water, run at 2500rpm / min for 15min to nucleate; run at 1000rpm / min for 50min to grow and form; Polish at 500rpm / min for 30min, add dry mixture powder with a mass fraction of 16%, and adjust the morphology.
[0054] (3) Dry the semi-finished ceramsite product at 105°C for 45 minutes, control the moisture to less ...
Embodiment 3
[0059] Formula: 87% mass fraction, 200-mesh low-quality bauxite 900°C light-fired material, the composition after light-fired is shown in Table 3.
[0060] Table 3 Composition of bauxite after light burning
[0061]
[0062] Additives, mass fraction 12%. Purity>99% water-soluble starch.
[0063] Dispersant, mass fraction 1.0% sodium polyacrylate.
[0064] Process:
[0065] (1) Low-quality bauxite is lightly burned at 900°C, ball milled to refine it to 200 mesh, and 12% of additives and 1.0% of dispersant are added by mass fraction and mixed uniformly to obtain a mixture;
[0066] (2) Add 90% of the mixture to the EIRICH vertical granulator for granulation, add 17% of atomized water, run at 5000rpm / min for 20min to nucleate; run at 2500rpm / min for 60min to grow and form; Polish at 1000rpm / min for 25min, add dry mixture powder with a mass fraction of 10%, and adjust the morphology.
[0067] (3) Dry the semi-finished ceramsite product at 105°C for 45 minutes, control the ...
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