Meta-stable vanadium oxide cathode materials for rechargeable magnesium battery
A magnesium storage battery and cathode technology, applied in vanadium oxide, battery electrodes, secondary batteries, etc., can solve problems such as reducing the energy density of batteries
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[0089] By ball milling V at 370 rpm in an Ar atmosphere 2 o 5 and P 2 o 5 Materials 20 hr to prepare the test materials listed in Table 1. Balls and jars for milling synthesis made of ZrO 2 production. After ball milling, the samples were annealed into a metastable phase and a thermodynamically stable phase, respectively, under an atmosphere of ambient air.
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[0091] image 3 shows a thermodynamically stable crystalline V 2 o 5 :P 2 o 5 (75:25 molar ratio), amorphous V 2 o 5 :P 2 o 5 (75:25 molar ratio), metastable V 2 o 5 :P 2 o 5 (75:25 molar ratio) and crystal V 2 o 5 The XRD pattern. After preparing the amorphous material as above, the metastable phase V was obtained by annealing at 325 °C for 5 h 2 o 5 :P 2 o 5 (75:25 molar ratio), and crystalline V was obtained by annealing at 450 °C for 5 h 2 o 5 :P 2 o 5 (75:25 molar ratio).
[0092] Figure 4 shows the thermodynamically stable crystalline V 2 o 5 :P 2 o 5 (75:25 molar ratio),...
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