A kind of high-performance water-in-oil base drilling fluid and preparation method thereof
A water-in-oil drilling fluid, oil-water-based technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of poor suspension ability and high temperature resistance, increased filtration loss, and high oil solubility, Achieve good plugging, reduce high temperature and high pressure filtration loss, and improve high temperature resistance.
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Embodiment 1
[0041] Take 30g of oxidized pitch with a softening point of 140.3°C and 70g of coal tar pitch with a softening point of 141.2°C, mix and heat to a molten state. Take 45g of styrene-butadiene rubber powder and preheat at 100°C for 25 minutes. Put the melted high softening point asphalt in the watering can, evenly spray the high softening point asphalt on the preheated granules, and stir while spraying. After spraying, it was left to stand at 130° C. for 35 minutes, and cooled to room temperature. Then place it in a freezer to freeze (freezing temperature -30°C, freezing time: 14 hours). After taking it out, put it into a vibrating sieve, and add 7g of cetyltrimethylammonium chloride. Use 80-mesh standard sieve as the bottom of the sieve, vibrate and pulverize for 35 seconds, and get the modified high softening point asphalt composition particles under the sieve.
[0042] First, measure 5# white oil (oil-water ratio 70:30) with a measuring cylinder, put it into a container wi...
Embodiment 2
[0044] Take 50g of oxidized pitch with a softening point of 152.6°C and 50g of coal tar pitch with a softening point of 150.2°C, mix them and heat them to a molten state. Take 38g of nitrile rubber powder and preheat at 95°C for 20 minutes. Put the melted high softening point asphalt in the watering can, evenly spray the high softening point asphalt on the preheated granules, and stir while spraying. After spraying, it was left to stand at 145° C. for 30 minutes, and then cooled to room temperature. Then place it in a freezer to freeze (freezing temperature -35°C, freezing time: 10 hours). Put into vibrating sieve after taking out, add 6.2g calcium lignosulfonate. Use a 100-mesh standard sieve as the bottom of the sieve, vibrate and pulverize for 25 seconds, and get the modified high softening point asphalt composition particles under the sieve.
[0045] First, measure 4# white oil (oil-water ratio 75:25) with a measuring cylinder, put it into a container with a stirring de...
Embodiment 3
[0047] Take 40g of oxidized pitch with a softening point of 168.2°C and 60g of coal tar pitch with a softening point of 170.5°C, mix and heat to a molten state. Take 56g of butyl rubber powder and preheat at 110°C for 20 minutes. Put the melted high softening point asphalt in the watering can, evenly spray the high softening point asphalt on the preheated granules, and stir while spraying. After spraying, it was left to stand at 155° C. for 30 minutes, and cooled to room temperature. Then place it in a freezer to freeze (freezing temperature -25°C, freezing time: 11 hours). After taking it out, put it into a vibrating sieve, and add 5.8g of sodium lignosulfonate. Use 80-mesh standard sieve as the bottom of the sieve, vibrate and pulverize for 40 seconds, and get the modified high softening point asphalt composition particles under the sieve.
[0048] First, measure 3# white oil (oil-water ratio 65:35) with a measuring cylinder, put it into a container with a stirring device...
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