Antibacterial fiber with washing resistance and preparation method thereof and antibacterial textile fabric and preparation method thereof
An antibacterial fiber and washing resistance technology, applied in the field of fibers, can solve the problems of not long-lasting antibacterial effect, insufficient fiber strength, and complicated preparation methods, and achieve the effects of superior antibacterial performance, simple production method and huge application potential.
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Embodiment 1
[0024] The nano-silver particle solution that mass concentration is 5% is diluted to 50ppm, regulates pH=7, cotton fiber is immersed in the nano-silver particle solution of 50ppm 10min with bath ratio 1: 10, makes nano-silver adsorb on the cotton fiber, then puts Put into the drier and carry out spin-drying treatment to obtain the cotton fiber of adsorption nano-silver; Then soak the cotton fiber of adsorption nano-silver into the cellulose xanthate solution (bath ratio 1: 5) that viscosity is 1000CPas and continue 10min, then Dry it in a spinner, then soak it in 5g / L sulfuric acid for 15 minutes, the bath ratio is 1:10, take it out, wash it with hot water and cold water, then dry it with a spinner at high speed, dry it with hot air, and shape it. The antibacterial fiber of the present invention.
Embodiment 2
[0026] Dilute the nano-silver solution with a mass concentration of 5% to 25ppm, adjust pH=8, immerse the cotton fiber in the solution for 30min with a bath ratio of 1:20, make the nano-silver adsorb on the cotton fiber, and then put it into a spin dryer Carry out spin-drying treatment to get the cotton fiber of adsorption nano-silver; Then soak the cotton fiber of adsorption nano-silver into the cellulose xanthate sodium solution (bath ratio 1: 10) of 5000CPas viscosity and continue 20min, then carry out spin-off in spinner. Dry, then soak it in 15g / L sulfuric acid for 30min, the bath ratio is 1:20, finally take it out and wash it with hot water, cold water, dehydration, drying, and setting to obtain the antibacterial fiber of the present invention.
Embodiment 3
[0028] Dilute the nano-silver solution with a mass concentration of 5% to 100ppm, adjust pH=8, immerse the cotton fiber in the solution with a bath ratio of 1:5 for 15 minutes, make the nano-silver adsorb on the cotton fiber, and then put it into a spin dryer The cotton fiber that adsorbs nano-silver is obtained by spinning and drying in the middle; then soak the cotton fiber that adsorbs nano-silver into the sodium cellulose xanthate solution with a viscosity of 50000CPas for 50min, the bath ratio is 1:15, and then spins in a spinning machine. dry, then soak it in a 30g / L sulfuric acid bath for 10min, the bath ratio is 1:10, and finally take it out and wash it with hot water, cold water, dehydration, and dry to obtain the antibacterial fiber of the present invention.
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