A kind of water-soluble high-efficiency concrete rosin resin air-entraining agent and preparation method thereof

A technology of rosin resin and concrete, which is applied in the preparation of water-soluble high-efficiency concrete rosin air-entraining agent, and in the field of water-soluble high-efficiency concrete rosin air-entraining agent. Effect of hydrophobic association, good gas stability

Active Publication Date: 2018-04-24
西藏五色石建材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The above technologies have not given specific guidance on how to make the concrete air-entraining agent have good water solubility, good air-entraining, foam stabilization, and dispersion performance

Method used

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  • A kind of water-soluble high-efficiency concrete rosin resin air-entraining agent and preparation method thereof
  • A kind of water-soluble high-efficiency concrete rosin resin air-entraining agent and preparation method thereof
  • A kind of water-soluble high-efficiency concrete rosin resin air-entraining agent and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Embodiment 1: The water-soluble high-efficiency concrete rosin air-entraining agent of the present invention is made from the raw materials of the following components and mass fractions: 50 parts of rosin resin, 0.5 part of p-toluenesulfonic acid, unsaturated dibasic acid 10 parts, 20 parts of alkylphenol polyoxyethylene ether, 3 parts of triethanolamine, 162 parts of deionized water. The above-mentioned unsaturated dibasic acid is maleic anhydride. The above-mentioned alkylphenol polyoxyethylene ether is OP-10.

[0024] The preparation method of the described water-soluble high-efficiency concrete rosin air-entraining agent comprises the following process steps: 1. the weighed rosin resin is pulverized in a pulverizer according to the above-mentioned parts by mass, and then the pulverized rosin resin is put into a reaction kettle, and the temperature is raised. To 130 ° C, after the rosin resin is completely melted, add p-toluenesulfonic acid into the reaction kettle...

Embodiment 2

[0025] Embodiment 2: The water-soluble high-efficiency concrete rosin air-entraining agent of the present invention is made from the raw materials of the following components and mass fractions: 50 parts of rosin resin, 0.5 part of p-toluenesulfonic acid, unsaturated dibasic acid 12 parts, 25 parts of alkylphenol polyoxyethylene ether, 5 parts of triethanolamine, 180 parts of deionized water. The above-mentioned unsaturated dibasic acid is fumaric acid. The above-mentioned alkylphenol polyoxyethylene ether is OP-15.

[0026] The preparation method of the described water-soluble high-efficiency concrete rosin air-entraining agent comprises the following process steps: 1. the weighed rosin resin is pulverized in a pulverizer according to the above-mentioned parts by mass, and then the pulverized rosin resin is put into a reaction kettle, and the temperature is raised. To 130 ° C, after the rosin resin is completely melted, add p-toluenesulfonic acid into the reaction kettle acc...

Embodiment 3

[0027] Embodiment 3: The water-soluble high-efficiency concrete rosin air-entraining agent of the present invention is made from the raw materials of the following components and mass fractions: 60 parts of rosin resin, 0.5 part of p-toluenesulfonic acid, unsaturated dibasic acid 15 parts, 30 parts of alkylphenol polyoxyethylene ether, 5 parts of triethanolamine, 215 parts of deionized water. The above-mentioned unsaturated dibasic acid is maleic acid. The above-mentioned alkylphenol polyoxyethylene ether is Triton X-10.

[0028] The preparation method of the described water-soluble high-efficiency concrete rosin air-entraining agent comprises the following process steps: 1. the weighed rosin resin is pulverized in a pulverizer according to the above-mentioned parts by mass, and then the pulverized rosin resin is put into a reaction kettle, and the temperature is raised. To 135 ° C, after the rosin resin is completely melted, add p-toluenesulfonic acid into the reaction kettl...

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Abstract

The invention relates to a water-soluble high-efficiency concrete rosin air entraining agent and a preparation method thereof. The rosin air retraining agent is prepared from 50-70 parts of rosin resin, 0.5-1.0 part of p-methyl benzenesulfonic acid, 10-20 parts of unsaturated diacids, 20-40 parts of alkylphenol polyoxyethylene, 3-5 parts of triethanolamine and 160-250 parts of deionized water. The invention also provides the preparation method of the rosin air entraining agent. The air entraining agent has the advantages of good water solubility, good air entraining, bubble stabilizing and dispersing performances, convenience in construction, and good economic and practical property. A test result shows that the air entraining agent has good low-temperature dissolving performance, additive compatibility, air entraining performance and bubble stabilizing performance, and good concrete construction workability, is suitable for being used in roads, bridges, reservoirs, dikes, buildings and other concrete engineering, and is especially suitable for being used in concrete structures with high antifreeze durability requirements, such as water conservancy projects, maritime works, roads and bridges and other national large engineering, and road and bridge engineering in the north and other alpine regions.

Description

technical field [0001] The invention relates to a concrete air-entraining agent, in particular to a water-soluble high-efficiency concrete rosin air-entraining agent. The invention also relates to a preparation method of the water-soluble high-efficiency concrete rosin air-entraining agent. Background technique [0002] Concrete air-entraining agents commonly used in the market mainly include sulfonic acid air-entraining agents and rosin soap air-entraining agents. Among them, the air-entraining agent produced by alkylsulfonate air-entraining agent has a large volume and poor stability of the bubbles, which affects the apparent quality of the concrete after hardening. Rosin soap air-entraining agent has good air-entraining ability and good bubble stability. However, the solubility of rosin soap in aqueous solution is small, and its dilute solution is in the form of emulsion, which must be shaken before use; when used in winter, due to the drop in temperature, the solubilit...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B24/34C04B103/30C04B103/40C04B103/48
CPCC04B40/0039C04B2103/304C04B2103/408C04B2103/48C04B24/34C04B24/20C04B24/04C04B24/32C04B24/122C04B22/002
Inventor 刘昭洋倪涛徐艳军王进春郭家泉
Owner 西藏五色石建材有限公司
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