A kind of liquid carboxylate metal salt and its preparation method and application
The technology of metal carboxylate and zinc carboxylate is applied in the field of liquid metal carboxylate and its preparation to achieve the effects of improving reaction yield, improving thermal stability and anti-precipitation performance, and reducing acid value
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Embodiment 1
[0034] Preparation of liquid barium carboxylate salt:
[0035] Mix 200kg oleic acid, 100kg isooctanoic acid, 130kg barium hydroxide monohydrate, 40kg diethylene glycol butyl ether and 30kg polyethylene glycol 400, stir, slowly raise the temperature to 100-105°C, react for 2 hours, dehydrate under reduced pressure for 40 minutes, Filter, collect filtrate and make liquid barium carboxylate 445kg.
Embodiment 2
[0037] Preparation of liquid zinc carboxylate salt:
[0038] 100kg isooctanoic acid, 10kg p-tert-butylbenzoic acid, 30kg zinc oxide, 20kg dipropylene glycol methyl ether and 9kg polyethylene glycol fatty ether AEO 3 Mix and stir, slowly raise the temperature to 110-115°C, react for 3 hours, dehydrate under reduced pressure for 35 minutes, filter, collect the filtrate to obtain 160kg of liquid barium carboxylate salt.
Embodiment 3
[0040] Preparation of liquid barium zinc carboxylate:
[0041] Mix 200kg oleic acid, 100kg isooctanoic acid, 80kg barium hydroxide monohydrate, 20kg zinc oxide, 50kg diethylene glycol butyl ether and 18g polyethylene glycol octylphenyl ether Triton X-100, stir, and slowly heat up to 100 ~105°C, react for 2 hours, dehydrate under reduced pressure for 40 minutes, filter, collect the filtrate to obtain 340 kg of liquid barium zinc carboxylate.
[0042] In Examples 1 to 3, the influence of the type and amount of phase transfer catalyst (accounting for the weight percentage of the mixed acid) on the reaction process and product yield is shown in Table 1.
[0043] Table 1 The effect of different phase transfer catalyst types and addition amounts on the reaction process and product yield
[0044] catalyst
[0045] Note: "Blank" means that no phase transfer catalyst is added during the synthesis process, and the others are consistent with Examples 1-3.
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