Method for synthesizing SiC nanowire toughened multilayer structure SiC-C/C composite material
A nanowire toughening and multi-layer structure technology, which is applied in the field of SiC-C/C composite materials, can solve the problems of high temperature requirements and difficulty in preparing SiC and C multi-layer structures, achieving low cost and improving overall mechanical properties , The effect of simple preparation method
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Embodiment 1
[0030] (1) Take an appropriate amount of tetraethyl orthosilicate, absolute ethanol and deionized water and mix them in a beaker, stir for several hours, then add a few drops of hydrochloric acid, adjust the pH value to less than 7 to acidic, and finally stir in a water bath for several hours , to obtain silica sol. Tetraethyl silicate, absolute ethanol and deionized water 300:150:57ml
[0031] (2) Put the carbon fiber prefabricated body into the prepared sol and dip for 24 hours; take out the prefabricated body, put it in a constant temperature box and dry it for 12 hours, and the temperature of the constant temperature box is 60°C; finally take out the sample, and let the sample naturally drop to room temperature, The carbon felt-silicon xerogel system can be obtained.
[0032] (3) ① Put the impregnated and dried silica gel-carbon felt into the graphite fixture, fill it in the CVI furnace, evacuate the furnace body, pour in argon gas, adjust to normal pressure, repeat sever...
Embodiment 2
[0043] (1) Take an appropriate amount of tetraethyl orthosilicate, absolute ethanol and deionized water and mix them in a beaker, stir for several hours, then add a few drops of hydrochloric acid, adjust the pH value to less than 7 to acidic, and finally stir in a water bath for several hours , to obtain silica sol.
[0044] (2) Put the carbon fiber prefabricated body into the prepared sol and soak for 72 hours; take out the prefabricated body, put it in a constant temperature box and dry it for 24 hours, and the temperature of the constant temperature box is 80°C; finally take out the sample, and let the sample drop to normal temperature naturally, The carbon felt-silicon xerogel system can be obtained.
[0045] (3) ① Put the impregnated and dried silica gel-carbon felt into the graphite fixture, fill it in the CVI furnace, evacuate the furnace body, pour in argon gas, adjust to normal pressure, repeat several times, and put the furnace The air in the body is exhausted.
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