Preparation method of dendrobium freeze-dried powder

A technology of freeze-dried powder and Dendrobium powder, which is applied in the direction of freeze-dried transportation, medical preparations containing active ingredients, powder transportation, etc., which can solve the problems of content reduction and heat-sensitive nutrient destruction, and achieve fast absorption and no solvent pollution Or residual, the effect of simple preparation method

Inactive Publication Date: 2017-05-24
贵州健瑞安药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the processing process of Dendrobium in the market generally needs to go through four process steps: sorting, baking, curling and ho

Method used

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  • Preparation method of dendrobium freeze-dried powder
  • Preparation method of dendrobium freeze-dried powder

Examples

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Example Embodiment

[0031] The invention provides a preparation method of freeze-dried dendrobium powder, which comprises the following steps:

[0032] Step 1. Use ultra-high pressure and low temperature technology to break the walls of fresh Dendrobium raw materials;

[0033] Step 2: After the broken fresh Dendrobium raw materials are refined and mixed uniformly, vacuum freeze-drying is used to obtain Dendrobium powder; the vacuum freeze-drying process specifically includes: sequentially pre-freezing the refined and mixed Dendrobium raw materials , The first sublimation and the second sublimation;

[0034] Step three, the Dendrobium powder is subjected to ultrafine grinding treatment.

[0035] The preparation method of the freeze-dried Dendrobium powder of the present invention adopts ultra-high pressure and low temperature technology to break the wall, so that the cell wall and cell membrane of the fresh Dendrobium are lysed, the medicinal ingredients are fully released and the activity of the medicina...

Example Embodiment

[0055] Example 1

[0056] A preparation method of freeze-dried dendrobium powder includes the following steps:

[0057] Step 1: Acceptance of Dendrobium raw materials: Dendrobium copper-skinned Dendrobium is produced in Huaping County, Lijiang City, Yunnan, and is fresh Dendrobium.

[0058] Step two, selection and cleaning: select the dendrobium without damage and mildew, and remove the leaves; then rinse the dendrobium with pure water.

[0059] Step 3: Breaking the wall: using ultra-high pressure and low temperature technology to lyse the cell wall and cell membrane of Dendrobium, fully release the medicinal ingredients and maintain the activity of the medicinal ingredients, which can well protect the bright color of Dendrobium. The processing conditions of ultra-high pressure low temperature technology are: a certain volume of cold water is filled in an ultra-high pressure vessel, the pressure of the vessel is 450 MPa, the pressure is maintained for 1 min, and the temperature is 60 ...

Example Embodiment

[0069] Example 2

[0070] A preparation method of freeze-dried dendrobium powder includes the following steps:

[0071] Step 1: Acceptance of Dendrobium raw materials: Dendrobium sclerosus is produced in Ziyun County, Guizhou Province, and is fresh Dendrobium.

[0072] Step two, selection and cleaning: select the dendrobium without damage and mildew, and remove the leaves; then rinse the dendrobium with pure water.

[0073] Step 3: Breaking the wall: using ultra-high pressure and low temperature technology to lyse the cell wall and cell membrane of Dendrobium, fully release the medicinal ingredients and maintain the activity of the medicinal ingredients, which can well protect the bright color of Dendrobium. The ultra-high-pressure cryogenic technology processing conditions are: a certain volume of cold water is filled in an ultra-high-pressure vessel, the vessel pressure is 480MPa, the pressure is maintained for 2 minutes, and the temperature is 55°C.

[0074] Step 4. Refining and mix...

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Abstract

The invention provides a preparation method of dendrobium freeze-dried powder. The preparation method comprises the following steps: firstly, breaking walls of a dendrobium raw material by adopting an ultrahigh pressure low temperature technique; secondly, grinding the dendrobium raw material after the walls are broken into thick liquid and uniformly mixing, and carrying out vacuum freeze-drying, so that dendrobium powder is obtained, wherein the vacuum freeze-drying process concretely comprises that pre-freezing, primary sublimation and secondary sublimation are sequentially carried out on the dendrobium raw material after being ground into the thick liquid and uniformly mixed; and thirdly, carrying out superfine grinding on dendrobium powder. In the preparation method of the dendrobium freeze-dried powder, the ultrahigh pressure low temperature technique is adopted for breaking the walls, and the vacuum freeze-drying and the superfine grinding are combined, so that raw material utilization ratio is improved, the biological activity of functional substances in fresh dendrobium raw materials is hardly lost, and pharmaceutical values and health effects of the dendrobium raw materials are enhanced.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicine processing, in particular to a preparation method of dendrobium freeze-dried powder. Background technique [0002] Fresh medicine refers to the medicine made by processing the whole or part of the tissue of fresh plants or animals, or taking its juice. The method of using fresh medicine is not only decoction, but also natural juice. In the "Compendium of Materia Medica" of the Ming Dynasty, there were more than 1,100 prescriptions using fresh herbs, and the application of fresh herbs in ancient times reached a peak. In modern times, due to the high cost of cultivation, storage and transportation of fresh medicine, and the limitation of processing technology, it is difficult to keep fresh medicine fresh, which limits its clinical application. develop. At present, dry products are mainly used to replace fresh medicines in clinical practice, and the traditional processing techn...

Claims

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Application Information

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IPC IPC(8): A61K36/8984A61K9/19A61P37/04A61P1/14A61P39/02A61P35/00A61P39/00A61P39/06A23L33/00A23P10/40
Inventor 王雪张珍孙立新
Owner 贵州健瑞安药业有限公司
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