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A kind of preparation method of superhydrophobic polyethylene fiber film

A polyethylene fiber, super-hydrophobic technology, applied in spinning solution preparation, textile and papermaking, non-woven fabrics and other directions, can solve the problems of high cost, unsuitable for industrial application, long cycle, etc. Short, low-cost effects

Active Publication Date: 2020-01-10
ZHENGZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods are costly and long-term in the actual application process, and are not suitable for industrial application.

Method used

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  • A kind of preparation method of superhydrophobic polyethylene fiber film
  • A kind of preparation method of superhydrophobic polyethylene fiber film
  • A kind of preparation method of superhydrophobic polyethylene fiber film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The preparation method of the superhydrophobic polyethylene fiber film of this embodiment, the specific operation steps are:

[0030] 1) Preparation of ultra-high molecular weight polyethylene spinning solution: take ultra-high molecular weight polyethylene powder and add it to the organic solvent xylene, and dissolve it at 140°C for more than 10 minutes until the ultra-high molecular weight polyethylene powder is completely dissolved in xylene to obtain Mass concentration is 0.05% ultra-high molecular weight polyethylene solution;

[0031] 2) Spinning and film spinning: such as figure 1 As shown, a stirring rod is set above the oil bath, and two steel wire frames are fixed and fixed symmetrically under the stirring rod, and the ultra-high molecular weight polyethylene solution prepared in step 1) is transferred to the inner diameter of the cylinder placed in the oil bath. In a 35mm necked glass container, the volume of the ultra-high molecular weight polyethylene solu...

Embodiment 2

[0039] The preparation method of the superhydrophobic polyethylene fiber film of this embodiment, the specific operation steps are:

[0040] 1) Preparation of ultra-high molecular weight polyethylene spinning solution: take ultra-high molecular weight polyethylene powder and add it to the organic solvent xylene, and dissolve it at 140°C for more than 10 minutes until the ultra-high molecular weight polyethylene powder is completely dissolved in xylene to obtain A mass concentration of 0.01% ultra-high molecular weight polyethylene solution;

[0041] 2) Spinning and film spinning: set a stirring bar above the oil bath, and connect two steel wire frames symmetrically and symmetrically below the stirring bar, transfer the ultra-high molecular weight polyethylene solution prepared in step 1) to the oil bath, The wire frame is immersed in the ultra-high molecular weight polyethylene solution, the oil bath temperature is set to 110°C, the stirring rate is set to 800r / min, and the co...

Embodiment 3

[0045] The preparation method of the superhydrophobic polyethylene fiber film of this embodiment, the specific operation steps are:

[0046] 1) Preparation of ultra-high molecular weight polyethylene spinning solution: take ultra-high molecular weight polyethylene powder and add it to the organic solvent xylene, and dissolve it at 140°C for more than 10 minutes until the ultra-high molecular weight polyethylene powder is completely dissolved in xylene to obtain Mass concentration is 0.5% ultra-high molecular weight polyethylene solution;

[0047] 2) Spinning and film spinning: set a stirring bar above the oil bath, and connect two steel wire frames symmetrically and symmetrically below the stirring bar, transfer the ultra-high molecular weight polyethylene solution prepared in step 1) to the oil bath, The steel wire frame is immersed in the ultra-high molecular weight polyethylene solution, the oil bath temperature is set at 115°C, the stirring rate is set at 800r / min, and the...

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Abstract

The invention relates to the technical field of high-molecular material processing and specifically relates to a preparation method of a super-hydrophobic polyethylene fiber film. The method comprises following steps: preparing ultrahigh molecular weight polyethylene spinning solution having a mass concentration of 0.1 to 0.5%; at 105 to 115 DEG C and the stirring speed being larger than 600 r / min, using a steel wire frame to rotate a crystal to spin and spin films, wherein the diameter of the steel wire is 0.5 to 1mm and the length and width of the steel wire frame are 40mm and 17mm respectively; then drying. According to the method of the invention, UHMWPE super-hydrophobic polyethylene fiber film having the shish-kebab structure can be directly manufactured by means of a flow induced crystallization method and the UHMWPE super-hydrophobic polyethylene fiber film has the function of self cleaning and can perfectly imitate the self cleaning capability of lotus leaf surface ; the film has the function of oil water separation and can absorb oil on the surface of water and can be applied in preventing sea pollution. The operation method of the invention is simple and convenient; the method is low in cost and has short period and is suitable for the industrialized popularization.

Description

technical field [0001] The invention relates to the technical field of polymer material processing, in particular to a preparation method of a superhydrophobic polyethylene fiber film. Background technique [0002] Superhydrophobic surfaces have attracted research due to their properties of static contact angles greater than 150° and rolling angles less than 10°. In nature, many plant leaves and waterfowl feathers are superhydrophobic. The surface of these animals and plants generally secretes hydrophobic oil or wax, and the surface is very rough, and the contact angle with water can reach more than 150°. The lotus leaf is famous for its superhydrophobicity and self-cleaning, thanks to its special graded roughness: there is a layer of waxy nanostructure on the fine micro papillae structure, and the droplets will sit on the top of the papillae structure, so These leaves will exhibit excellent superhydrophobicity. At present, referring to the hydrophobic principle of natura...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D04H3/007D04H3/16D01D1/02
CPCD01D1/02D04H3/007D04H3/16
Inventor 刘宪虎孙双杰郑国强朱利亚代坤刘春太
Owner ZHENGZHOU UNIV
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