Interlayer filler material and laminate for touch panels
By using a combination of polyvinyl acetal and specific organic acids and plasticizers, combined with heating and pressure bonding technology, the problem of whitening of the interlayer filler material for touch panels and deterioration of the ITO film under high temperature and humidity is solved, achieving a high-low Poor followability and defoaming properties improve the durability and transparency of the material.
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Embodiment 1~24、 comparative example 1~30
[0058] (1) Preparation of polyvinyl butyral
[0059] 2700 mL of ion-exchanged water, 300 g of polyvinyl alcohol having an average degree of polymerization of 3200 and a degree of saponification of 88.0 mol % were charged into a reactor equipped with a stirring device, and heated and dissolved while stirring to obtain a solution. Next, 35% by weight of hydrochloric acid was added as a catalyst to this solution so that the concentration of hydrochloric acid became 0.6% by weight, and after adjusting the temperature to 15° C., 14.2 g of n-butyraldehyde (n-BA) was added with stirring. Then, when 186 g of n-butyraldehyde (n-BA) was added, white granular polyvinyl butyral precipitated. After 15 minutes from the precipitation, 35% by weight of hydrochloric acid was added so that the concentration of hydrochloric acid became 3.9% by weight, heated to 45° C., and aged at 45° C. for 3 hours. Next, after the solution was cooled and neutralized, polyvinyl butyral was washed with water an...
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