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146 results about "Ethyleneglycol bis" patented technology

Bionic exosome for anti-inflammatory and repair as well as preparation method and application of bionic exosome

The invention relates to a bionic exosome for anti-inflammation and repair as well as a preparation method and application thereof, and belongs to the field of cosmetics. The bionic exosome provided by the invention comprises a membrane structure and an internal load phase, the membrane structure comprises a phospholipid bilayer, a stabilizer and a targeting ligand; the internal load phase comprises a solvent and an active component; the phospholipid bilayer is composed of phospholipid compounds; preferably, at least one of the distearoyl phosphatidyl ethanolamine-polyethylene glycol 2000 and the 1, 2-dioleoyl-sn-glycerol-3-phosphoethanolamine is adopted as the phospholipid compound, and at least one of the distearoyl phosphatidyl ethanolamine-polyethylene glycol 2000 and the 1, 2-dioleoyl-sn-glycerol-3-phosphoethanolamine is adopted as the phospholipid compound; at least one of cholesterol, phytosphingosine and sodium stearoyl glutamate is preferably adopted as a stabilizer, so that the stabilizer of the obtained bionic exosome is improved, and the bionic exosome has the advantages of high encapsulation efficiency, good encapsulation efficiency stability, simplicity in operation, excellent anti-inflammatory and repairing effects and the like.
Owner:GUANGZHOU FANZHIRONG COSMETICS CO LTD +1

Particle temporary plugging agent and preparation method thereof

The invention discloses a granular temporary plugging agent and a preparation method thereof. The granular temporary plugging agent comprises the following components in percentage by mass: 17-23% of acrylamide; 1-2% of a comonomer; 0.2 to 0.27% of a first cross-linking agent; 5-10% of polyvinyl alcohol; 1-2% of a second cross-linking agent; 0.06 to 0.12% of an initiator; 0.01%-0.02% of an initiating auxiliary agent; 3-6% of a modified nano blending material; 0.3%-0.6% of a dispersing agent; and the balance of distilled water. Wherein the first cross-linking agent is one or more of ethylene glycol dimethacrylate, polyethylene glycol diacrylate and trimethylolpropane trimethacrylate; the second cross-linking agent is one or two of a beta-cyclodextrin-boron complex and a glycerol-boron complex; the modified nano blending material is soda lime silicate modified by surface activation-silane coupling modification, and is in the form of hollow microspheres. The in-seam temporary plugging agent system provided by the invention is low in density, good in plugging performance and excellent in degradation performance.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Ethylene glycol diacetate preparation reaction equipment

The invention relates to the technical field of ethylene glycol diacetate preparation, and discloses ethylene glycol diacetate preparation reaction equipment, which comprises a tower body, a reboiler and a condenser, the top of the tower body is connected with the condenser, the bottom of the tower body is connected with the reboiler, a tower plate is installed in the tower body, the tower plate is driven to rotate in the tower body, and the tower plate has a first state and a second state, in the first state, the tower plate is of an L-shaped structure and is horizontally arranged, and in the second state, the tower plate is of a linear structure and is inclined downwards; the tower plate provided by the invention can be kept in the second state in the cleaning process, and when water flows on the tower plate in the second state, the tower plate is of a linear structure, so that the tower plate in the state does not influence impact force generated by flowing of the water, and the tower plate can be smoothly flushed.
Owner:SHANDONG LUYANG NEW MATERIAL TECH CO LTD

Solid shaving aid composition

The present disclosure describes a razor cartridge including a housing having a front edge and a rear edge; shaving blades disposed between the front edge and the rear edge; and at least one shaving bar disposed in front of the blade(s) and / or rear of the blade(s) which includes a solid shaving aid composition that includes, relative to the total weight of the solid shaving aid composition: about 15 wt.-% to about 48 wt.-% of a soap base including of one or more fatty acid salts having from about 8 to about 24 carbon atoms and optionally one or more fatty acids having from about 8 to about 24 carbon atoms, at least about 35 wt.-% of one or more polyols including from ˜2 to ˜8 carbon atoms; the polyol selected from a group including glycerol, sorbitol, ethylene glycol, diethylene glycol, propylene glycol, dipropylene glycol, tripropylene glycol, methylpropane diol glycol.
Owner:BIC VIOLEX SINGLE MEMBER SA

Hydrogel patch for wound sealing and repairing as well as preparation method and application of hydrogel patch

The invention provides a wound sealing and repairing hydrogel patch and a preparation method thereof. The hydrogel patch is provided with an independent adhesion layer and an adhesion layer and anti-adhesion layer combination. The adhesive layer is prepared from gelatin, N-acryloylated amino acid, acrylic acid-N-succinimide ester, 2-hydroxy-4 '-(2-hydroxyethoxy)-2-methyl propiophenone and water through ultraviolet light crosslinking; the anti-adhesion layer is prepared from methacryloyl ethyl sulphobetaine, polyethylene glycol diacrylate, 2-hydroxy-4 '-(2-hydroxyethoxy)-2-methyl propiophenone and water through ultraviolet light crosslinking. The hydrogel patch can be used for sealing and repairing wounds of various tissues (such as skin tissues, liver tissues and stomach tissues), the healing time is shortened, the healing effect is improved, the healing time of a skin incision can be shortened from 14 days to 10 days, the hydrogel patch is superior to other treatment modes according to macroscopic photos and related slices, and the hydrogel patch has a good application prospect. And no-injury healing can be realized.
Owner:CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY CHINESE ACADEMY OF SCIENCES

Self-crystallization type amino acid cleansing cream composition and preparation method thereof

The invention discloses a self-crystallization type amino acid cleansing cream composition and a preparation method thereof. Comprising the following components in percentage by weight: 20%-40% of glycerol, 15%-25% of cocoyl glycinate, 1%-10% of cocoyl hydrolyzed collagen potassium, 0.1%-5% of sodium lauroamphoacetate, 0.1%-3% of citric acid, 0.1%-3% of sodium methyl cocoyl taurate, 0.1%-3% of sodium chloride, 0.1%-3% of sodium lauroyl glutamate, 0.1%-3% of ethyoxyl diethylene glycol, 0.1%-3% of propylene glycol laurate, 0.1%-3% of PEG-150 stearate, 0.1%-3% of ethylene glycol distearate, 0.0%-2% of 1, 3-propylene glycol distearate, 0.0%-2% of 1, 3-propylene glycol distearate and the balance of water. The cleaning agent is prepared from the following components in percentage by weight: 0.0 to 2 percent of 1, 2-hexanediol, 0.0 to 2 percent of p-hydroxyacetophenone and The self-crystallization type cleansing cream composition disclosed by the invention is high in crystallization point, good in thermal stability, mild and low in irritation, and has the effects of moisturizing and promoting cell proliferation, and the overall performance is improved.
Owner:NANJING HUASHI NEW MATERIAL CO LTD

A mxene material and a preparation method thereof

This invention belongs to the field of two-dimensional material preparation technology, and provides an MXene material and its preparation method. The preparation method of the MXene material includes: mixing a MAX phase precursor to be etched with an organic halide reagent and a morphology modifier, performing a solvothermal etching reaction, and after the reaction, washing and drying the resulting product to obtain the MXene material; wherein the organic halide reagent is triethylamine trihydrofluoride, triethylamine hydrochloride, or dichloroethylamine hydrochloride, and the morphology modifier is ethylene glycol, dimethyl sulfoxide, or cyclohexane. The method of this invention can effectively control the microstructure and pore structure of the MXene material.
Owner:YANAN UNIV

Polyelectrolyte hydrogel coating with strong substrate binding performance and method of manufacturing the same

A polyelectrolyte hydrogel coating with strong substrate binding performance and a method of manufacturing the same are provided. The method includes: 1) activating a substrate by applying oxygen plasma; and 2) dissolving a polycationic polymer, a polymeric monomer, a silane coupling agent and an initiator to obtain a precursor solution, vacuumizing the precursor solution to remove air bubbles, applying the vacuumized precursor solution to a surface of the substrate activated by the oxygen plasma, and performing an in-situ polymerization and curing process under nitrogen or rare gas atmosphere. The polymeric monomer includes at least one of: acrylamide, acrylic acid, hydroxyethyl methacrylamide, 2-acrylamido-2-methyl-1-propanesulfonic acid, polyethylene glycol (diol) diacrylate, 2-methacryloxyethylphosphocholine, 3-[[2-(Methacryloyloxy)ethyl]dimethylammonio]propane-1-sulfonate, and 3-[[2-(methacryloyloxy)ethyl]dimethylammonium] propionate. The silane coupling agent has a carbon-carbon double bond functional group.
Owner:ZHEJIANG UNIV

A method and device for recovering caustic pot residue for ethylene carbonate production of ethylene glycol

In order to overcome the problems of high recovery price, high energy consumption and low utilization rate of the existing kettle residue for the production of ethylene glycol by ethylene carbonate alcoholysis method, the application provides a kettle residue recovery method and device for the production of ethylene glycol by ethylene carbonate alcoholysis method, and the application provides a kettle residue recovery method for the production of ethylene glycol by ethylene carbonate, which comprises the following steps: under the conditions of temperature 150-250 DEG C and pressure 0.6-2 MPa, the ethylene glycol in the kettle residue produced by the preparation of ethylene glycol by ethylene carbonate alcoholysis method is converted into diethylene glycol under the catalysis of alkali metal salt catalyst, and after the reaction is completed, the kettle residue is a mixture of ethylene glycol, diethylene glycol, triethylene glycol and salt, the mixture is purified, and ethylene glycol and diethylene glycol are recovered; the economic benefit is improved, the rectification separation operation is simplified, the equipment investment and the overall energy consumption are reduced, and the utilization rate of ethylene glycol kettle residue is improved.
Owner:HUIZHOU CAPCHEM CHEM CO LTD

Nd-Fe-B magnetic powder auxiliary agent and application thereof and preparation method of Nd-Fe-B magnet

The invention discloses an Nd-Fe-B magnetic powder auxiliary agent, application of the Nd-Fe-B magnetic powder auxiliary agent and a preparation method of an Nd-Fe-B magnet. The Nd-Fe-B magnetic powder auxiliary agent comprises a solid auxiliary agent and a liquid auxiliary agent, the solid additive comprises 45-80 parts by weight of an ethylene amide compound, 22-45 parts by weight of saturated fatty alcohol and 0.03-0.8 part by weight of molybdenum disulfide; the liquid auxiliary agent is prepared from 0.5 to 1.5 volume parts of carboxylic ester compound and 0.5 to 3 volume parts of boric acid ester compound; the carboxylic ester compound is selected from isooctyl oleate, ethyl oleate, methyl palmitate, polyethylene glycol dioleate, methyl myristate, methyl stearate and methyl laurate; the borate compound is selected from triisopropyl borate, triethanolamine borate, tributyl borate, triethyl borate, trimethyl borate, tripropyl borate and triisobutyl borate. The Nd-Fe-B magnetic powder auxiliary agent can effectively improve the magnetic performance of a neodymium-iron-boron magnet.
Owner:BAOTOU RESEARCH INSTITUTE OF RARE EARTHS

Method for producing polyacrylamide by kneading machine

The invention discloses a method for producing polyacrylamide by a kneading machine. The method comprises the following steps: (1) forming a mixed solution A from acrylamide, 2-acrylamido-2-methyl propane sodium sulfonate, polyethylene glycol diacrylamide, a chain transfer auxiliary agent and water; (2) forming a cationic monomer solution from a cationic monomer, a cosolvent and water; (3) forming a mixed solution B from a part of the mixed solution A and a part of the cation mixed solution; (4) forming a mixed solution C from a redox initiator, an azo initiator and water; (5) putting the residual mixed solution A into a polymerization reaction kettle, introducing nitrogen to remove oxygen, regulating the temperature, adding the mixed solution C, stirring to react, cooling, adding the cationic monomer solution and the mixed solution C, stirring to react, cooling, adding the mixed solution B and the mixed solution C, stirring to react, heating, preserving heat and standing to obtain colloid; and (6) transferring the colloid into a kneading machine, vacuumizing and kneading. The produced polyacrylamide is high in molecular weight and concentrated in distribution, and has good dissolution and flocculation performance.
Owner:PACMC MFG CO LTD

Temperature-sensitive slow-release medical auxiliary material and preparation method thereof

ActiveCN120695250ABandagesPolymer scienceSwelling ratio
The invention discloses a temperature-sensitive slow-release medical auxiliary material and a preparation method of the temperature-sensitive slow-release medical auxiliary material, and belongs to the technical field of medical auxiliary materials. Comprising the following components: 1-2% w / v of acrylamide hydroxyethyl chitosan, 5-15% w / v of polyethylene glycol diacrylate, 1-6% w / v of N-methyl acrylate caprolactam, 0.05-2% w / v of an initiator, 0.01-0.5% w / v of a cross-linking agent and the balance of a PBS (Phosphate Buffer Solution), the acrylamide hydroxyethyl chitosan is modified by chitosan hydroxyl group and ethyl group; the N-methyl acrylate caprolactam monomer provided by the invention effectively improves the temperature sensitivity of the temperature-sensitive polymer auxiliary material; the acrylamide hydroxyethyl chitosan can reduce the swelling ratio and slow down the drug release; the polyethylene glycol diacrylate can be a crosslinking monomer of the temperature-sensitive polymer auxiliary material, meanwhile, an ether bond is introduced to improve the biocompatibility of the temperature-sensitive polymer auxiliary material, and the temperature-sensitive slow-release medical auxiliary material which is low in drug slow-release rate and responds to the temperature of a human body is prepared by combining the polyethylene glycol diacrylate, the ether bond and the temperature-sensitive polymer auxiliary material.
Owner:GUANGDONG NANWO MEDICAL TECHNOLOGY CO LTD

A method and device for recovering ethylene in ethylene gas containing seal oil

The present invention provides a method and a device for recovering ethylene in ethylene gas containing seal oil, relating to the technical field of ethylene recovery. In the present invention, ethylene glycol diacetate is used as a solvent to absorb ethylene in the ethylene gas containing seal oil, and the obtained ethylene-rich liquid is analyzed, so as to realize the efficient separation and recovery of ethylene. The recovery rate of ethylene is high, and the recovered ethylene can be directly used in the production of vinyl acetate by the ethylene method, greatly reducing the consumption of ethylene raw materials in the process of producing vinyl acetate by the ethylene method. Moreover, ethylene glycol diacetate is produced as a by-product in the process of producing vinyl acetate by the ethylene method. In the present invention, ethylene glycol diacetate (EGDA) is used as a solvent, and no new impurities are introduced.
Owner:EAST CHINA UNIV OF SCI & TECH

Synergistic extraction and separation method for gold in high-concentration gold-containing solution

The invention belongs to the technical field of precious metal extraction, and particularly relates to a synergistic extraction separation method for gold in a high-concentration gold-containing solution, diethylene glycol dibutyl ether, tributyl phosphate and sulfonated kerosene are mixed to obtain a synergistic extraction agent, and the synergistic extraction agent is used for extracting a gold-containing chlorination leaching solution to obtain a gold-containing extraction phase; in the synergistic extractant, the molar ratio of diethylene glycol dibutyl ether to tributyl phosphate is (5-35): 1; in the synergistic extraction agent, the concentration of diethylene glycol dibutyl ether is 0.5 to 3.5 mol / L; according to the method provided by the invention, the extraction agent is selected, and the extraction process parameters such as the ratio of the extraction agent, the ratio of an organic phase to water, the extraction temperature and the extraction stage number are adjusted, so that a good extraction and separation effect on gold can be obtained, and efficient separation of gold in the high-concentration gold-containing solution is realized. The method is good in synergistic effect, good in gold and impurity separation effect and high in efficiency.
Owner:CENT SOUTH UNIV

Gel material for treating keloid capable of reducing generation of lactic acid

The invention discloses a keloid treatment gel material capable of reducing lactic acid generation, and belongs to the technical field of keloid treatment. The material is prepared by the following steps: firstly, carrying out esterification on 9-oxabicyclo [3.3. 1] nonane-2, 6-diol and S-allyl-L-cysteine to obtain an intermediate A, and then carrying out Schiff base reaction on the intermediate A and 5-methoxy heliotropin to obtain an intermediate B containing double bonds; then, copolymerizing with methylacryloylated chitosan and polyethylene glycol diacrylate under photo-initiation to form a cross-linked network structure; finally, active ingredients such as quercetin-3-O-glucuronide and luteolin-3 '-glucuronide are included, and auxiliary materials such as a humectant and a preservative are added, so that the composition is prepared. The gel has a slow release function, can effectively inhibit glycolysis, reduce lactic acid generation, scavenge free radicals and regulate inflammation and fibrosis microenvironment, has good biocompatibility and oxidation response drug release characteristics, and is suitable for prevention and treatment of keloids.
Owner:TONGJI HOSPITAL ATTACHED TO TONGJI MEDICAL COLLEGE HUAZHONG SCI TECH

A concrete brightener and preparation method thereof

ActiveCN117164272BActive agentCarbon nanotube
The present invention discloses a concrete brightener and a preparation method thereof, comprising the following components by weight: 100-140 parts of a hydrophilic unsaturated carboxylic acid ester, 70-100 parts of a lipophilic unsaturated carboxylic acid ester, 0.5-2 parts of a modified single-walled carbon nanotube, 8-14 parts of ethylene glycol distearate, 5-9 parts of an imidazoline compound, 2-7 parts of a polyglycerol fatty acid ester, 6-12 parts of a nonionic surfactant, 18-35 parts of a fluorocarbon surfactant, 5-9 parts of a molecular regulator, 3-8 parts of an initiator, and 664-783 parts of water. The present invention can be used in conjunction with an admixture during concrete prefabrication. After use, the concrete brightener has a smooth surface and more uniform color of cement products, can maintain a long-lasting brightening effect, and can achieve strong adsorption and dispersion effects on cement, thereby improving the strength and surface hardness of cement products and enhancing the surface brightness, smoothness, and wear resistance of cement products. Furthermore, the present invention has mild preparation conditions and does not use any organic solvents during the synthesis process, making it safe and environmentally friendly.
Owner:YUNNAN SENBO CONCRETE ADMIXTURE CO LTD

A method for determining the content of ethylene glycol and diethylene glycol in laundry beads by gas chromatography

The present invention belongs to the technical field of chemical detection, and discloses a method for determining the content of ethylene glycol and diethylene glycol in laundry beads by gas chromatography. The detection method of the present invention comprises the following steps: weighing the laundry beads, dissolving them in methanol after crushing, fixing the volume, and then ultrasonically extracting, centrifuging, filtering, and diluting to obtain a sample solution to be tested; subjecting the sample solution to be tested to gas chromatography-mass spectrometry detection to determine whether it contains ethylene glycol and diethylene glycol; conducting gas chromatography detection to obtain the area of ​​the chromatographic peaks of ethylene glycol and diethylene glycol, bringing them into the standard working curve, and obtaining the concentration of ethylene glycol and diethylene glycol, and calculating the content of ethylene glycol and diethylene glycol in the laundry beads. The present invention can accurately measure the content of ethylene glycol and diethylene glycol components, promote a more standardized market for laundry beads products, reduce the addition of components toxic to the human body, such as ethylene glycol and diethylene glycol, in production, and better protect the rights and interests of consumers.
Owner:ZHONGQING INSPECTION & CERTIFICATION (TAIYUAN) CO LTD

Essence mixture, fragrant PVC leather thereof and preparation method of fragrant PVC leather

The invention belongs to the technical field of artificial leather, and particularly relates to an essence mixture, fragrant PVC (polyvinyl chloride) leather and a preparation method thereof. The essence premix is added into the formula for modification, so that the prepared artificial leather can release fragrance for a long time. The essence premix comprises essence methyl dihydrojasmonate and tridecanedioic acid cyclic ethylene glycol diester, and the mass ratio of the methyl dihydrojasmonate to the tridecanedioic acid cyclic ethylene glycol diester is 1: (1-4). A small amount of essence is added in the formula, the fragrance emitted by the essence can effectively shield the smell of the raw materials, special equipment is not needed for production, special treatment is not needed, and the product cost can be effectively reduced; the fragrant PVC leather prepared by the invention can effectively control the volatilization amount and the volatilization speed of the fragrance of the essence. The fragrance duration is effectively prolonged, and the effect of slowly releasing fragrance for a long time is achieved.
Owner:SAGE-ONF AUTOMOTIVE INTERIOR MATERIAL (JIANGSU) CO LTD

A microemulsion containing fluroxypyr-meptyl and clopyralid and a method for preparing the same

The present application relates to the technical field of pesticide preparation, in particular to a microemulsion containing fluroxypyr-isooctyl and aminoclopidol and a preparation method thereof, which is composed of the following components in percentage by mass: fluroxypyr-isooctyl 1-15%, aminoclopidol 1-15%, composite emulsifier 10-22%, co-emulsifier 5-11%, composite solvent 15-28%, antifreezing agent 2-6%, stabilizer 0.5-2.5%, and deionized water, with the total being 100%. The composite emulsifier is composed of dioctyl sodium sulfosuccinate and triphenyl ethenyl phenol polyoxyethylene ether phosphate triethanolamine salt, the composite solvent is composed of N,N-dimethyl decanamide and ethylene glycol diacetate, the stabilizer is composed of epoxidized soybean oil and citric acid, the co-emulsifier is dipropylene glycol methyl ether, and the antifreezing agent is glycerol. The microemulsion containing fluroxypyr-isooctyl and aminoclopidol and the preparation method thereof effectively solve a plurality of technical problems in the compounding process of the two active ingredients and have significant technical advantages.
Owner:LANXI JINGHANG BIOTECHNOLOGY CO LTD

Polymer drug carrier for treating cat tinea

The invention belongs to the field of external medicines for pets, and provides a macromolecular medicine carrier for treating cat tinea, which is prepared by adopting a collaborative design of core-shell nanogel particles and a double-state antibacterial component and through stepwise reaction of hexamethylene diisocyanate, polyethylene glycol, polyethylene glycol diamine and a silane coupling agent. A core-shell structure with the particle size of 100-350 nm and the shell thickness of 5-30 nm is formed through water dispersion emulsification and silane hydrolytic condensation, and a Si-O-Si bond fixed state and non-covalent releasable state antibacterial mechanism is constructed by combining polyhexamethylene biguanide hydrochloride. According to the invention, the powerful antibacterial property of the minimal inhibitory concentration of 0.2-3.00 mg / mL to pathogenic dermatophyte is realized, a low-viscosity processing window and skin-friendly pH value are kept at 5.5-7.5, the coupling problem of high load, long-acting washing resistance, rapid effect and continuous inhibition and film-forming adhesion durability of an external preparation is solved, and the preparation has wide application value.
Owner:SUZHOU XINJIALI MEDICAL TECH CO LTD

Preparation method of ethylene sulfate

The invention provides a preparation method of ethylene sulfate in order to solve the problems that in the prior art, ethylene glycol, thionyl chloride, sodium hypochlorite and ruthenium trichloride are used for preparing ethylene sulfate, cost is high, operation is complex, generated waste brine has adverse effects on the environment, and sodium ions and chloride ions in ethylene sulfate easily exceed standards. Comprising the following steps: mixing and heating concentrated sulfuric acid and ethylene glycol to carry out esterification reaction, continuously bubbling and introducing sulfur trioxide gas into a mixed solution composed of the concentrated sulfuric acid and the ethylene glycol in the esterification reaction process, and after the esterification reaction is finished, carrying out post-treatment to obtain the ethylene sulfate. According to the preparation method of the ethylene sulfate provided by the invention, the cost is low on the basis of obtaining higher yield, the technological process is simple to operate, the reaction conditions are milder, a dehydrating agent is not needed, sulfur trioxide can be recycled, three wastes are less, sodium ion and chloride ion impurities are not contained, and the purity of the ethylene sulfate is high.
Owner:JIANGSU HICOMER NEW MATERIAL CO LTD

A process for the preparation of 1,1-ethylene glycol diacetate

This invention discloses a method for preparing 1,1-ethylene glycol diacetate, characterized by: using acetic acid and vinyl acetate as raw materials, reacting under reflux at 80-85°C in the presence of a catalyst; after the reaction is complete, turning off the heating, adding sodium acetate to the reaction vessel, continuing the reaction to neutralize the catalyst; after the reaction is complete, separating the solid from the mixture, and concentrating the liquid phase to obtain the target product 1,1-ethylene glycol diacetate. The catalyst is at least one selected from concentrated sulfuric acid, methanesulfonic acid, and p-toluenesulfonic acid. The raw materials are safe and environmentally friendly, inexpensive, and can be reacted under normal pressure, requiring less sophisticated equipment, facilitating industrial production, and yielding high purity.
Owner:CHONGQING RES INST OF CHEM IND

Granular temporary plugging agent and preparation method thereof

The invention discloses a particle temporary plugging agent and a preparation method thereof, wherein the particle temporary plugging agent comprises the following components according to mass percentage: acrylamide: 17-23%; comonomer: 1-2%; first crosslinking agent: 0.2-0.27%; polyvinyl alcohol: 5-10%; second crosslinking agent: 1-2%; initiator: 0.06-0.12%; initiator aid: 0.01-0.02%; modified nano-blended material: 3-6%; dispersant: 0.3-0.6%; the rest is distilled water; wherein the first crosslinking agent is one or more of ethylene glycol dimethacrylate, polyethylene glycol diacrylate, and trimethylolpropane trimethacrylate; the second crosslinking agent is one or two of β-cyclodextrin-boron complex and glycerol-boron complex; the modified nano-blended material is a soda lime silicate modified by surface activation-silane coupling modification, and the form is hollow microspheres. The invention realizes providing a low-density, good plugging performance, and excellent degradation performance of the temporary plugging agent system in the seam.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

A 50 / 50 hybrid polyester resin for powder coating and its preparation method

This invention relates to a polyester resin for 50 / 50 blended powder coatings. This polyester resin is obtained by reacting raw materials including glycerin black lead, ethylene glycol, diethylene glycol, terephthalic acid, 4,4'-biphenyl dicarboxylic acid, succinic acid, and pyromellitic dianhydride. The resulting product exhibits good impact resistance, a gloss level generally above 92%, and other properties such as adhesion that basically meet the application requirements of 50 / 50 blended powder coatings. Due to the comprehensive utilization of the effective components of glycerin black lead, it has the advantages of low cost and outstanding environmental performance.
Owner:HUANGSHAN YUANRUN NEW MATERIAL TECH CO LTD

Anti-fog glass and preparation method thereof

The invention provides anti-fog glass and a preparation method thereof. The anti-fog glass comprises a glass substrate, a bonding layer and an anti-fog layer, wherein the bonding layer is arranged between the anti-fog layer and the glass substrate; the coating of the anti-fog layer comprises the following components in parts by weight: 70-90 parts of a first monomer, 5-15 parts of a second monomer, 3-6 parts of a cross-linking agent and 5-10 parts of a photoinitiator; the first monomer comprises one or a combination of more than two of hydroxyethyl methylacrylate, polyethylene glycol diacrylate, N-hydroxymethyl acrylamide, methacrylamide, N-isopropylacrylamide and N, N-dimethylacrylamide; the second monomer is prepared from one or a combination of more than two of trifluoroethyl methacrylate, methyl methacrylate, butyl acrylate, ethylene glycol dimethacrylate, glycidyl methacrylate, benzyl methacrylate and 2-acrylic acid-2-hydroxy-3-phenoxy propyl ester. The anti-fog glass disclosed by the invention has the advantages of anti-fog property, moisture resistance, salt fog resistance and wear resistance.
Owner:FUYAO GLASS IND GROUP CO LTD

Processes for making 1,2-diacetoxyethane from monoethylene glycol by reactive distillation

Disclosed herein are various embodiments pertaining to continuous processes for making ethylene glycol diacetate, also known as 1,2-diacetoxyethane, by esterification of monoethylene glycol to 2-hydroxyethyl acetate and the esterification of 2-hydroxyethyl acetate to ethylene glycol diacetate. Various embodiments herein use reactive distillation in processes promising enhanced economic viability in the production of high-quality ethylene glycol diacetate.
Owner:NEW PRODUCT INNOVATIONS LLC

Polymer based cellular labeling, barcoding and assembly

To provide a method for synthesizing a capped cationic polymer.SOLUTION: Provided is a method that includes: (a) contacting poly(ethylene glycol) diacrylate monomers and 3-amino-1-propanol to form a poly(ethylene glycol) diacrylate / 3-amino-1-propanol cationic polymer by Michael Addition, wherein the molar ratio of the poly(ethylene glycol) diacrylate monomers to 3-amino-1-propanol is greater than 1, and the cationic polymer is acrylate-terminated; and (b) contacting terminal acrylate groups of the cationic polymer with capping molecules comprising amine groups to form the capped cationic polymer by Michael Addition, wherein the capped cationic polymer comprises no acrylate groups.SELECTED DRAWING: Figure 1A
Owner:CHILDRENS HOSPITAL MEDICAL CENT CINCINNATI

A preparation method and application of a 3D printed silicon-based ceramic core

The present invention provides a method for preparing a 3D printed silicon-based ceramic core, and the method is as follows: After mixing 1,6-ethylene glycol diacrylate, epoxy acrylate, trimethylolpropane triacrylate and polyurethane acrylate, add 2,4,6-trimethylbenzoyl-ethoxy-phenyl phosphine oxide, oleic acid and dispersant BYK-111, and stir and mix to obtain a premixed liquid; After mixing fused quartz powder, white fused alumina and zirconium silicate, add metallic Si powder to obtain a mixture; Add the premixed liquid to the mixture, ball mill to obtain a ceramic slurry, prepare a ceramic core blank by 3D printing, clean, dry, and then calcine to obtain a 3D printed silicon-based ceramic core. It also provides an application for manufacturing hollow blades. The 3D printed silicon-based ceramic core prepared by the present invention has excellent mechanical properties and can be used for manufacturing hollow blades.
Owner:CHANGAN UNIV

Uniconazole membrane modified suspending agent as well as preparation method and application thereof

PendingCN119111511AImprove dwarfing control effectpromote growthBiocidePlant growth regulatorsBiotechnologyCellulose
The invention discloses a uniconazole membrane modified suspending agent as well as a preparation method and application thereof. The uniconazole membrane modified suspending agent comprises the following components in percentage by mass: 10% of uniconazole, 2-3% of carboxymethylcellulose, 0.05% of maleic anhydride grafted isobutylene, 0.5-0.8% of a stabilizer, 0.3% of poloxamer, 0.1% of a preservative, 3-5% of ethylene glycol, 3-5% of N, N-dimethylformamide, 0.2% of an organic silicon defoaming agent, 8% of a film-forming agent and the balance of water. Researches show that compared with a 10% uniconazole suspending agent, the uniconazole membrane modified suspending agent provided by the invention can significantly improve the plant dwarfing regulation effect, and has a significant dwarfing effect on eucalyptus, moso bamboo, schima superba and conic.
Owner:HEYUAN POWER SUPPLY BUREAU GUANGDONG POWER GRID CO LTD

Oil-in-water emulsion cosmetics

To provide an oil-in-water emulsion cosmetic with high moisturizing effect and viscosity stability. [Solution] An oil-in-water emulsion cosmetic comprising (A) a hydrophilic nonionic surfactant, (B) a higher aliphatic alcohol having 12 or more carbon atoms, (C) a polyethylene glycol difatty acid ester with a polymerization number of 20 or less of polyoxyethylene glycol, (D) an oil, and (E) water.
Owner:SHISEIDO CO LTD