A kind of reinforced concrete rust inhibitor and preparation method thereof
A technology of reinforced concrete and rust inhibitor, applied in the field of rust inhibitor, can solve the problems of inability to popularize and apply green rust inhibitor, narrow source of raw materials, poor rust inhibitor effect, etc. The effect of improving the rust inhibition effect
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[0024] A preparation method for reinforced concrete rust inhibitor, which comprises steps:
[0025] (a) Take 1 kg of dehydrated mushrooms, crush them to 80-100 mesh, add 8L of 0.1mol / L NaOH solution, and soak for 8-12 hours;
[0026] (b) heating the soaked oyster mushroom to 60-65° C., keeping it for 1 hour and filtering while it is hot to obtain filter residue;
[0027] (c) Wash the filter residue until neutral, add 10mol / L NaOH solution, heat to 120-130°C, keep for 2 hours, filter while it is hot to obtain a filtrate, cool the filtrate to normal temperature, and filter the resulting white precipitate;
[0028] (d) Wash the white precipitate with water until neutral, add 1 liter of 8.82mol / LH 2 o 2 100 ml of 0.1mol / L acetic acid, heated at 50-60°C for 1 hour, raised the temperature to 100°C, kept for 10 minutes, and cooled to obtain the oyster mushroom extract;
[0029] (e) Add 0.1mol vanillin to the extract of Pleurotus ostreatus, control the temperature at 55-60°C to rea...
Embodiment 1
[0040] Weigh various raw materials according to the ratio of mass and number stated below
[0041] Modified oyster mushroom extract 30 parts
[0042] Calcium gluconate 1 part
[0043] Sodium dodecylbenzenesulfonate 2 parts
[0044]67 parts of water
[0045] The preparation method of described reinforced concrete rust inhibitor is as follows:
[0046] (1) Take 1KG dehydrated mushrooms, crush them to 80-100 mesh, add 8L 0.1mol / L NaOH solution, and soak for 8-12 hours; heat the soaked oyster mushrooms to 60-65°C and keep for 1 hour; Filtrate hot to obtain filter residue;
[0047] (2) Wash the filter residue obtained in step (1) until neutral, add 10mol / L NaOH solution, heat to 120-130°C, keep it for 2 hours, filter while it is hot, and obtain the filtrate; cool the filtrate to room temperature, white Precipitation occurs, filtered;
[0048] (3) Wash the white precipitate filtered in step (2) until neutral, add 8.82mol / LH 2 o 2 1L, 100ml of 0.1mol / L acetic acid, heat at 50...
Embodiment 2
[0052] Weigh various raw materials according to the ratio of mass and number stated below
[0053] Modified oyster mushroom extract 60 parts
[0054] Calcium gluconate 4 parts
[0055] Sodium dodecylbenzene sulfonate 6 parts
[0056] 30 parts of water
[0057] The preparation method of described reinforced concrete rust inhibitor is as follows:
[0058] (1) Take 1KG dehydrated mushrooms, grind them to 80-100 mesh, add 8L 0.1mol / L NaOH solution, soak for 8-12 hours; heat the soaked oyster mushrooms to 60°C and keep for 1 hour; filter while hot , get filter residue;
[0059] (2) Wash the filter residue obtained in step (1) until neutral, add 10mol / L NaOH solution, heat to 120-130°C, keep it for 2 hours, filter while it is hot, and obtain the filtrate; cool the filtrate to room temperature, white Precipitation occurs, filtered;
[0060] (3) Wash the white precipitate filtered in step (2) until neutral, add 8.82mol / LH 2 o 2 1L, 100ml of 0.1mol / L acetic acid, heat at 50-60°...
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