Preparation method of antipersprant deodorant
An antiperspirant and mass fraction technology, applied in the field of skin care products, can solve problems such as uncomfortable use, unfavorable health, inflammation of use, etc., and achieve the effects of improved function, reduced force, and soft skin
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[0025] A preparation method of antiperspirant, comprising the steps of:
[0026] (1) Take fresh pomegranate peel and mix it with 30% hydrochloric acid solution and 50% methanol solution at a mass ratio of 1:15~18:8~14, extract at 20~25°C for 1~2h, Concentrate under reduced pressure at 50-55°C, vacuum degree 0.08-0.1MPa, freeze-dry, dry the extract, and set aside;
[0027] (2) Add cornstarch to water at a mass ratio of 3:10, stir in a constant temperature water bath at 25~30°C, adjust the pH to 7.5~8, then add 2~4% of the water quality of octenyl succinic anhydride, and filter with suction. Take the filter residue and wash it with distilled water, dry it, take the dry filter residue and add water to mix according to the mass ratio of 2:9, adjust the pH to 5~5.5, add aluminum sulfate with 20~30% of the filter residue quality, react for 0.5~1h, suction filter, take suction filter The product was washed with distilled water and ethanol in turn, dried to obtain a dry product, and ...
Embodiment 1
[0031] Corn starch: purchased from COFCO Biochemical Energy Co., Ltd.
[0032] Wheat gluten protein: protein content 70%, purchased from Bob's Red Mill Natural Foods.
[0033] A preparation method of antiperspirant, comprising the steps of:
[0034] (1) Take fresh pomegranate peel and add 30% hydrochloric acid solution and 50% methanol solution at a mass ratio of 1:15:8, mix them, and extract at 20°C for 1 hour. At 50°C, the vacuum degree is 0.08 Concentrate under reduced pressure at MPa, freeze-dry, dry the extract, and set aside;
[0035](2) Add cornstarch to water at a mass ratio of 3:10, stir in a constant temperature water bath at 25°C, adjust the pH to 7.5, then add 2% octenyl succinic anhydride to the water quality, filter with suction, and wash the filter residue with distilled water. Dry, take the dry filter residue and add water to mix according to the mass ratio of 2:9, adjust the pH to 5, add aluminum sulfate with 20% of the quality of the filter residue, react f...
Embodiment 2
[0039] Corn starch: purchased from COFCO Biochemical Energy Co., Ltd.
[0040] Wheat gluten protein: 75% protein, purchased from Bob's Red Mill Natural Foods.
[0041] A preparation method of antiperspirant, comprising the steps of:
[0042] (1) Take fresh pomegranate peel and add 30% hydrochloric acid solution and 50% methanol solution at a mass ratio of 1:16:12 to mix, extract at 23°C for 1 hour, and at 53°C, the vacuum degree is 0.09 Concentrate under reduced pressure at MPa, freeze-dry, dry the extract, and set aside;
[0043] (2) Add cornstarch to water at a mass ratio of 3:10, stir in a constant temperature water bath at 27°C, adjust the pH to 7.9, then add 3% octenyl succinic anhydride to the water quality, filter with suction, and wash the filter residue with distilled water. Drying, take the dry filter residue and mix it with water according to the mass ratio of 2:9, adjust the pH to 5.3, add aluminum sulfate with a mass of 25% of the filter residue, react for 0.7h,...
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