Fluid loss reducer for drilling fluid and preparation method thereof
A fluid loss control agent and drilling fluid technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of poor resistance to saturated brine, poor temperature resistance, and high manufacturing costs, and achieve strong anti-pollution ability. , The effect of low manufacturing cost and low production cost
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[0019] The present invention also provides a preparation method of the fluid loss control agent for drilling fluid, comprising the steps of: taking AMPS, N-isopropylacrylamide, acrylamide, pyrrolidone, p-styrenesulfonic acid according to the corresponding weight percentage Raw material of sodium, ammonium persulfate and sodium bisulfite; first mix AMPS, N-isopropylacrylamide and acrylamide evenly, add appropriate amount of sodium hydroxide solution, then add pyrrolidone, sodium p-styrenesulfonate and persulfuric acid Ammonium and sodium bisulfite, mixed evenly and heated to 45°C-55°C, reacted for 5-7h, dried and pulverized.
[0020] In order to shorten the preparation time and ensure product quality, further, mix AMPS, N-isopropylacrylamide, and acrylamide evenly, add an appropriate amount of sodium hydroxide solution, and then add pyrrolidone, sodium p-styrenesulfonate, and ammonium persulfate , Sodium bisulfite, mix evenly and heat to 50°C, react for 6h, dry and pulverize. ...
Embodiment 1
[0023] Take: 20 parts of AMPS, 40 parts of N-isopropylacrylamide, and 10 parts of acrylamide are evenly mixed, adding an appropriate amount of sodium hydroxide solution, and then adding 20 parts of pyrrolidone, 9.5 parts of sodium p-styrenesulfonate, and 0.4 parts of ammonium persulfate 1. 0.1 part of sodium bisulfite, mix evenly and heat to 50°C, react for 6 hours, dry and pulverize. The "fluid loss reducer for drilling fluid" can be obtained.
Embodiment 2
[0025] Take: 40 parts of AMPS, 20 parts of N-isopropylacrylamide, and 20 parts of acrylamide are evenly mixed, add an appropriate amount of sodium hydroxide solution, and then add 10 parts of pyrrolidone, 9.5 parts of sodium p-styrenesulfonate, and 0.2 parts of ammonium persulfate 1. 0.3 parts of sodium bisulfite, mix evenly and heat to 45°C, react for 7 hours, dry and pulverize. The "fluid loss reducer for drilling fluid" can be obtained.
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