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Fluid loss reducer for drilling fluid and preparation method thereof

A fluid loss control agent and drilling fluid technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of poor resistance to saturated brine, poor temperature resistance, and high manufacturing costs, and achieve strong anti-pollution ability. , The effect of low manufacturing cost and low production cost

Active Publication Date: 2021-08-24
四川泓华油气田工程科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] Existing fluid loss additives for drilling fluids have the following problems: ① poor temperature resistance, especially 200 degrees Celsius; ② poor resistance to saturated brine
[0005] Although the fluid loss reducer for drilling fluid described in the above invention patent has good ability to resist saturated brine and high temperature, its components are complicated and the manufacturing cost is relatively high

Method used

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  • Fluid loss reducer for drilling fluid and preparation method thereof

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preparation example Construction

[0019] The present invention also provides a preparation method of the fluid loss control agent for drilling fluid, comprising the steps of: taking AMPS, N-isopropylacrylamide, acrylamide, pyrrolidone, p-styrenesulfonic acid according to the corresponding weight percentage Raw material of sodium, ammonium persulfate and sodium bisulfite; first mix AMPS, N-isopropylacrylamide and acrylamide evenly, add appropriate amount of sodium hydroxide solution, then add pyrrolidone, sodium p-styrenesulfonate and persulfuric acid Ammonium and sodium bisulfite, mixed evenly and heated to 45°C-55°C, reacted for 5-7h, dried and pulverized.

[0020] In order to shorten the preparation time and ensure product quality, further, mix AMPS, N-isopropylacrylamide, and acrylamide evenly, add an appropriate amount of sodium hydroxide solution, and then add pyrrolidone, sodium p-styrenesulfonate, and ammonium persulfate , Sodium bisulfite, mix evenly and heat to 50°C, react for 6h, dry and pulverize. ...

Embodiment 1

[0023] Take: 20 parts of AMPS, 40 parts of N-isopropylacrylamide, and 10 parts of acrylamide are evenly mixed, adding an appropriate amount of sodium hydroxide solution, and then adding 20 parts of pyrrolidone, 9.5 parts of sodium p-styrenesulfonate, and 0.4 parts of ammonium persulfate 1. 0.1 part of sodium bisulfite, mix evenly and heat to 50°C, react for 6 hours, dry and pulverize. The "fluid loss reducer for drilling fluid" can be obtained.

Embodiment 2

[0025] Take: 40 parts of AMPS, 20 parts of N-isopropylacrylamide, and 20 parts of acrylamide are evenly mixed, add an appropriate amount of sodium hydroxide solution, and then add 10 parts of pyrrolidone, 9.5 parts of sodium p-styrenesulfonate, and 0.2 parts of ammonium persulfate 1. 0.3 parts of sodium bisulfite, mix evenly and heat to 45°C, react for 7 hours, dry and pulverize. The "fluid loss reducer for drilling fluid" can be obtained.

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Abstract

The invention discloses a fluid loss reducer for drilling fluid which can realize resistance to salt to saturation, more than 5% of calcium, strong anti-pollution ability and low manufacturing cost while ensuring high temperature resistance and a preparation method thereof. The fluid loss reducer used in the drilling fluid consists of 20% to 40% of AMPS, 20% to 40% of N-isopropylacrylamide, 10% to 20% of acrylamide, and 10% to 20% of pyrrolidone in terms of weight percentage. 20%, 8% to 11% of sodium p-styrene sulfonate, 0.2% to 0.4% of ammonium persulfate, and 0.1% to 0.3% of sodium bisulfite. The preparation method comprises the steps of uniformly mixing AMPS, N-isopropylacrylamide, and acrylamide, adding an appropriate amount of sodium hydroxide solution, then adding pyrrolidone, sodium p-styrenesulfonate, ammonium persulfate, and sodium bisulfite, and mixing Evenly heat to 45°C~55°C, react for 5~7h, dry and pulverize. The fluid loss reducer for drilling fluid has high salt resistance and high temperature resistance, and at the same time has a calcium resistance of more than 5%, and strong pollution resistance; meanwhile, the preparation method is simple, convenient for production and low in production cost.

Description

technical field [0001] The invention relates to a fluid loss reducer for drilling fluid and a preparation method thereof, in particular to a modified resin fluid loss reducer for drilling fluid and a preparation method thereof. Background technique [0002] Well-known: Filtrate reducer for drilling fluid (fluidloss reducers), also known as fluid loss reducer, is an external additive used to reduce the liquid-phase fluid loss of drilling fluid or the loss of liquid-phase leakage into the formation. agent. Classified by chemical composition, fluid loss reducers can be divided into minerals, natural organic substances and their modified substances (such as lignite lye, pregelatinized or modified starch), synthetic organic substances (such as methyl cellulose and polyester) Acrylates), etc. [0003] The existing fluid loss reducers for drilling fluids have the following problems: ① poor temperature resistance, especially 200 degrees Celsius; ② poor resistance to saturated brin...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/035C09K8/03
CPCC09K8/032C09K8/035
Inventor 刘乾忠
Owner 四川泓华油气田工程科技有限公司