A kind of synthetic method of sns2/mn3o4 three-dimensional multilevel structure and the product obtained therefrom
A synthesis method and three-dimensional technology, applied in chemical instruments and methods, tin compounds, manganese oxide/manganese hydroxide, etc., can solve the problems of less theoretical guidance and complicated experimental process, and achieve easy reaction process, simple equipment and uniformity Good results
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Embodiment 1
[0034] 1.1 Add 0.4781 g of tin chloride pentahydrate, 0.6659 g of thioacetamide and 0.0590 g of p-phenylenediamine to 30 mL of absolute ethanol, and stir to obtain a transparent solution;
[0035] 1.2 Transfer the above transparent solution to the reaction kettle, and react in a closed manner at 160 °C for 18 h, after centrifugation and washing, the SnS 2 flower-like self-assembly;
[0036] 1.3 Add 0.0952 g of SnS 2 The flower-like self-assembly was dispersed into a mixed solvent of 12.5 mL of glycerol and 12.5 mL of water, and 0.2312 g of PVP, 0.1249 g of manganese chloride tetrahydrate and 0.3580 g of sodium acetate trihydrate were added to dissolve completely, and a mixture was obtained. liquid;
[0037] 1.4 Transfer the above mixed solution to the reaction kettle, and react in a closed manner at 180 °C for 16 h, after centrifugation and washing, the SnS 2 / Mn 3 o 4 Three-dimensional multilevel structure.
[0038] The XRD result of the product is as follows figure 1...
Embodiment 2
[0040] 2.1 Add 0.2444 g of tin chloride pentahydrate, 0.4399 g of thioacetamide and 0.0437 g of p-phenylenediamine into 30 mL of absolute ethanol, and stir to obtain a transparent solution;
[0041] 2.2 Transfer the above transparent solution to the reaction kettle, and react in a closed manner at 170 °C for 19 h, after centrifugation and washing, the SnS 2 flower-like self-assembly;
[0042] 2.3 Add 0.1600 g of SnS 2 The flower-like self-assembly was dispersed into a mixed solvent of 12.5 mL of glycerol and 12.5 mL of water, and 0.3108 g of PVP, 0.1050 g of manganese chloride tetrahydrate and 0.6976 g of sodium acetate trihydrate were added to dissolve completely, and a mixture was obtained. liquid;
[0043] 2.4 Transfer the above mixed solution to the reaction kettle, and react in a closed manner at 190 °C for 6 h, after centrifugation and washing, the SnS 2 / Mn 3 o 4 Three-dimensional multilevel structure. The skeleton structure of the three-dimensional hierarchical s...
Embodiment 3
[0045] 3.1 Add 0.4993 g of tin chloride pentahydrate, 0.5564 g of thioacetamide and 0.0770 g of p-phenylenediamine into 30 mL of absolute ethanol, and stir to obtain a transparent solution;
[0046] 3.2 Transfer the above transparent solution to the reaction kettle, seal the reaction at 150 °C for 7 h, centrifuge and wash to obtain SnS 2 flower-like self-assembly;
[0047] 3.3 Add 0.0800 g of SnS 2 The flower-like self-assembly was dispersed into a mixed solvent of 12.5 mL of glycerol and 12.5 mL of water, and 0.2282 g of PVP, 0.1399 g of manganese chloride tetrahydrate and 0.2586 g of sodium acetate trihydrate were added to dissolve completely, and a mixture was obtained. liquid;
[0048] 3.4 Transfer the above mixed solution to the reaction kettle, and react in a closed manner at 170 °C for 17 h. After centrifugation and washing, SnS 2 / Mn 3 o 4 Three-dimensional multilevel structure. The skeleton structure of the three-dimensional hierarchical structure is composed of...
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