Transition metal complex used as phosphorescent material, preparation method of transition metal complex and application of transition metal complex
A transition metal and phosphorescent material technology, applied in luminescent materials, compounds containing elements of Group 8/9/10/18 of the periodic table, palladium organic compounds, etc., can solve the problems of small color adjustment range and achieve high luminous efficiency , the effect of simple operation
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Embodiment 1
[0037] The synthesis of iridium complex Ir12, the reaction equation is as follows:
[0038] (1) Synthesis of chlorine-bridged dimers
[0039]
[0040] (2) Target synthesis
[0041]
Embodiment 2
[0043] The synthesis of iridium complex Ir10, the reaction equation is as follows:
[0044] (1) Synthesis of chlorine-bridged dimers
[0045]
[0046] (2) Target synthesis
[0047]
Embodiment 3
[0049] The synthesis of iridium complex Ir7, reaction equation is as follows:
[0050] (1) Synthesis of chlorine-bridged dimers
[0051]
[0052] (2) Target synthesis
[0053]
[0054] The transition metals involved in the complexes prepared in Examples 1-3 are represented by Ir, and Pd or Pt can also be used to prepare transition metal complexes, and the reaction principle and process are the same as those of Ir.
[0055] Such as figure 1 As shown, the structure of an organic electroluminescent device (OLED) includes a glass substrate 1, an anode layer 2, a hole injection layer 3, a hole transport layer 4, a light emitting layer 5, an electron transport layer 6, and an electron injection layer sequentially stacked and combined. layer 7 and cathode layer 8. The iridium phosphorescent material prepared by the present invention is applied in the light-emitting layer of the OLED, and Table 1 shows the composition of each layer of the OLED in application examples 1-3.
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