Transition metal complex as phosphorescent material, and preparation method and application of transition metal complex
A transition metal and phosphorescent material technology, applied in luminescent materials, platinum-based organic compounds, compounds containing elements of Group 8/9/10/18 of the periodic table, etc., can solve the problems of small color adjustment range and achieve luminous efficiency High, easy-to-use effects
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Embodiment 1
[0036] The synthesis of iridium complex Ir10, the reaction equation is as follows:
[0037] (1) Synthesis of chlorine-bridged dimers
[0038]
[0039] (2) Target synthesis
[0040]
Embodiment 2
[0042] The synthesis of iridium complex Ir7, reaction equation is as follows:
[0043] (1) Synthesis of chlorine-bridged dimers
[0044]
[0045] (2) Target synthesis
[0046]
Embodiment 3
[0048] The synthesis of iridium complex Ir9, the reaction equation is as follows:
[0049] (1) Synthesis of chlorine-bridged dimers
[0050]
[0051] (2) Target synthesis
[0052]
[0053] The transition metals involved in the complexes prepared in Examples 1-3 are represented by Ir, and Pd or Pt can also be used to prepare transition metal complexes, and the reaction principle and process are the same as those of Ir.
[0054] Such as figure 1 As shown, the structure of an organic electroluminescent device (OLED) includes a glass substrate 1, an anode layer 2, a hole injection layer 3, a hole transport layer 4, a light emitting layer 5, an electron transport layer 6, and an electron injection layer sequentially stacked and combined. layer 7 and cathode layer 8. The iridium phosphorescent material prepared by the present invention is applied in the light-emitting layer of the OLED, and Table 1 shows the composition of each layer of the OLED in application examples 1-3....
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