Rapid heating distillation device in refining process of high-purity titanium tetrachloride

A technology of high-purity titanium tetrachloride and distillation device, which is applied in the field of rapid heating distillation device, can solve the problems of reducing the working efficiency of the distillation device, affecting the normal use of the distillation device, and easy to make mistakes in the sealing of installation workers, so as to facilitate disassembly and maintenance, prevent Air leakage, increase the effect of firmness

Active Publication Date: 2018-12-04
河南龙兴钛业科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a high-purity titanium tetrachloride refining process in the rapid heating distillation device, to solve the existing distillation device proposed in the above-mentioned background technology in use, because the steps are loaded down with trivial details when the sealing cover is sealed, and need Repeatedly check the airtightness, the installation workers are prone to make mistakes when sealing, which affects the normal use of the distillation device and reduces the working efficiency of the distillation device

Method used

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  • Rapid heating distillation device in refining process of high-purity titanium tetrachloride

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Embodiment 1

[0020] Example 1: see figure 1 , figure 2 , image 3 and Figure 4 , a rapid heating distillation device in the refining process of high-purity titanium tetrachloride, comprising a feed pipe 1, a sealing cover 2, a distillation device main body 4, a slag discharge pipe 7, a sealing cover 11 and a support provided on the lower surface of the distillation device main body 4 mechanism, the top of the main body 4 of the distillation device is provided with a fixing mechanism, and the fixing mechanism includes a first L-shaped fixing block 3, a nut 12, a threaded rod 13, a second L-shaped fixing block 14, a second arc-shaped groove 15, and a fixing hole 16 , limit groove 17, limit block 18, sliding groove 19 and first arc-shaped groove 26, feed pipe 1 is installed and fixed on the upper surface of sealing cover 2, and sealing cover 2 is installed and placed on the top of distillation device main body 4, The slag discharge pipeline 7 is installed and fixed on the bottom of the m...

Embodiment 2

[0025] Example 2: see figure 2 , image 3 , Figure 4 and Figure 5 , a rapid heating distillation device in the refining process of high-purity titanium tetrachloride, comprising a feed pipe 1, a sealing cover 2, a distillation device main body 4, a slag discharge pipe 7, a sealing cover 11 and a support provided on the lower surface of the distillation device main body 4 mechanism, the top of the main body 4 of the distillation device is provided with a fixing mechanism, and the fixing mechanism includes a first L-shaped fixing block 3, a nut 12, a threaded rod 13, a second L-shaped fixing block 14, a second arc-shaped groove 15, and a fixing hole 16 , limit groove 17, limit block 18, sliding groove 19 and first arc-shaped groove 26, feed pipe 1 is installed and fixed on the upper surface of sealing cover 2, and sealing cover 2 is installed and placed on the top of distillation device main body 4, The slag discharge pipeline 7 is installed and fixed on the bottom of the ...

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Abstract

The invention discloses a rapid heating distillation device in a refining process of high-purity titanium tetrachloride. The device comprises a material inlet pipeline, a sealing cover, a distillationdevice main body, a residue discharging pipeline, a closing cover and a supporting mechanism arranged at the lower surface of the distillation device main body; and the top end of the distillation device main body is provided with a fixing mechanism, and the fixing mechanism comprises a first L-shaped fixing block, a nut, a threaded rod, a second L-shaped fixing block, a second arc-shaped groove,a fixing hole, limiting grooves, limiting blocks, sliding grooves and a first arc-shaped groove. According to the device disclosed by the invention, the limiting blocks slide in the limiting grooves,so that the second L-shaped fixing block is prevented from falling off and being lost from the interiors of the sliding grooves, and use costs of users are reduced; and the nut is rotated at the surface of the threaded rod in a clockwise direction, so that upward sliding of the second L-shaped fixing block in the sliding grooves is facilitated, tight bonding of the connection place of the sealingcover and the distillation device main body is realized, the sealing cover is convenient to install and place on the top end of the distillation device main body, and the sealing cover is convenientto disassemble and repair from the surface of the distillation device main body.

Description

technical field [0001] The invention belongs to the technical field of rapid heating distillation devices, in particular to a rapid heating distillation device in the refining process of high-purity titanium tetrachloride. Background technique [0002] In the refining process of titanium tetrachloride, according to the characteristics of the large difference between the high boiling point and low boiling point impurities in the crude titanium tetrachloride and the boiling point or relative volatility of titanium tetrachloride, the impurities are separated by distillation or rectification. Distillation is used to separate the high-boiling impurities that are easy to separate, and rectification is used to separate the difficult-to-separate low-boiling impurities. [0003] During the use of the existing distillation device, due to the cumbersome steps in sealing the sealing cover and the need to repeatedly check the airtightness, the installation workers are prone to make mista...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D3/32C01G23/02
CPCB01D3/32C01G23/024
Inventor 龙志王攀峰郜二芬程福建张苍南苗雷
Owner 河南龙兴钛业科技股份有限公司
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