A trans-electrically controlled light-adjustable film capable of adjusting near-infrared light transmittance and its preparation method
A technology of near-infrared light and light-adjustable film, which is applied in optics, nonlinear optics, instruments, etc., can solve the problems of restricting the adjustment of smart windows and the inability to adjust the transmittance of near-infrared light and visible light at the same time, and achieve the near-infrared film The light transmittance is intelligently controllable and the effect of improving the bonding strength
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Embodiment 1
[0051] step one:
[0052] 2.3g of vanadium dioxide powder (micron size, purchased from Alpha Aisha, with a purity of 99%) was dispersed in 10g of ethanol, and 0.45g of Disperbyk 180 was added as a dispersant during the dispersion process to stabilize the nanoparticles. Subsequently, the above-mentioned dispersion liquid was stirred with a roller ball mill at a rotation speed of 4200 rpm, and a nanoscale vanadium dioxide ethanol dispersion liquid was obtained after a duration of 4 hours. The dispersion liquid was left to stand for 2 days to obtain a stable vanadium dioxide nanoparticle dispersion liquid after removing the precipitate. Utilize ICP to carry out elemental analysis to above-mentioned dispersion liquid, record the massfraction of vanadium dioxide to be 15wt.%.
[0053] Step two:
[0054] The selected liquid crystals, polymerizable monomers, initiators, names and proportions of spacer particles are listed in Table 2. Mix the components in Table 2 according to the ...
Embodiment 2
[0062] In this example, a toluene dispersion of vanadium dioxide nanoparticles was used, with a mass fraction of 3%. Purchased from Hangzhou Jikang New Material Co., Ltd.
[0063] step one:
[0064] The selected liquid crystals, polymerizable monomers, initiators, names and proportions of spacer particles are listed in Table 3. Mix the components in Table 2 according to the ratio, and stir at room temperature to form an isotropic liquid, and mix well. The total mass of the mixture is 9.6 g.
[0065] Table 3. The proportioning of each material used in embodiment 2
[0066] name Proportion / % Dual frequency nematic liquid crystal material 60.2 polymerizable monomer 38.8 Initiator 0.5 20 micron spaced particles 0.5
[0067] Step two:
[0068] Add 13.3 g of the above-mentioned toluene dispersion of vanadium dioxide nanoparticles to the mixture in step 1, and sonicate for 10 minutes to disperse the nanoparticles evenly. Subsequently, it ...
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