A kind of fiber-reinforced composite thermal insulation material and preparation method thereof

A fiber-reinforced composite and thermal insulation material technology, applied in the field of thermal insulation materials, can solve the problems that thermal insulation materials do not have reflective energy and oxidation resistance, cannot meet the design and use requirements, and the heat resistance of materials is difficult to solve, and achieve good results. Antioxidant effect, no decline in mechanical properties, and improved compatibility

Active Publication Date: 2021-06-04
GUANGDONG HAILONG CONSTR TECH CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The advantages of organic materials are sufficient raw materials, low thermal conductivity of products, convenient construction, and mature technology. design requirements
And the existing thermal insulation materials do not have the function of reflecting energy and oxidation resistance, so it is necessary to design a thermal insulation material with high compressive strength, high tensile strength and low thermal conductivity, as well as reflecting energy and oxidation resistance. very necessary

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A fiber-reinforced composite thermal insulation material, the raw materials are 30 parts by weight of silica airgel powder, 15 parts of aluminum silicate fiber, 10 parts of aluminum solution, 5 parts of potassium hexatitanate whisker, electrospun poly 8 parts of vinylidene fluoride micro-nano fiber, 45 parts of modified sepiolite fiber, 35 parts of modified nano-alumina fiber and 1 part of aluminum dihydrogen phosphate;

[0032] The parts by weight of each raw material in the modified sepiolite fiber are 15 parts of sepiolite, 40 parts of hydrochloric acid, 3 parts of toluene, 1 part of N,N-dimethylformamide and 2 parts of flame retardant polymer;

[0033]The parts by weight of each raw material in the flame retardant polymer are 30 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 13 parts of amine, 5 parts of magnesium hydroxide, 1 part of dispersant, 3 parts of antioxidant and 15 parts of dimethyl sulfoxide;

[0034] The preparatio...

Embodiment 2

[0047] A fiber-reinforced composite thermal insulation material, the raw materials are 50 parts by weight of silica airgel powder, 35 parts of aluminum silicate fiber, 15 parts of aluminum solution, 8 parts of potassium hexatitanate whisker, electrospun poly 12 parts of vinylidene fluoride micro-nano fiber, 58 parts of modified sepiolite fiber, 39 parts of modified nano-alumina fiber and 6 parts of aluminum dihydrogen phosphate;

[0048] The parts by weight of each raw material in the modified sepiolite fiber are 23 parts of sepiolite, 60 parts of hydrochloric acid, 5 parts of toluene, 6 parts of N,N-dimethylformamide and 7 parts of flame retardant polymer;

[0049] The parts by weight of each raw material in the flame retardant polymer are 40 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 20 parts of amine, 8 parts of magnesium hydroxide, 1-6 parts of dispersant, 5 parts of antioxidant and 25 parts of dimethyl sulfoxide;

[0050] The pre...

Embodiment 3

[0063] A fiber-reinforced composite thermal insulation material, the raw materials are 75 parts by weight of silica airgel powder, 60 parts of aluminum silicate fiber, 20 parts of aluminum solution, 10 parts of potassium hexatitanate whisker, electrospun poly 15 parts of vinylidene fluoride micro-nano fiber, 65 parts of modified sepiolite fiber, 45 parts of modified nano-alumina fiber and 9 parts of aluminum dihydrogen phosphate;

[0064] The parts by weight of each raw material in the modified sepiolite fiber are 30 parts of sepiolite, 75 parts of hydrochloric acid, 7 parts of toluene, 8 parts of N,N-dimethylformamide and 10 parts of flame retardant polymer;

[0065] The parts by weight of each raw material in the flame retardant polymer are 45 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 25 parts of amine, 10 parts of magnesium hydroxide, 1-6 parts of dispersant, 8 parts of antioxidant and 30 parts of dimethyl sulfoxide;

[0066] The ...

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PUM

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Abstract

The invention discloses a fiber-reinforced composite heat-insulating material and a preparation method thereof. The raw materials are 30-75 parts of silica airgel powder, 5-10 parts of potassium hexatitanate whisker, electrospun poly 8-15 parts of vinylidene fluoride micro-nano fibers, 45-65 parts of modified sepiolite fibers, 35-45 parts of modified nano-alumina fibers and 1-9 parts of aluminum dihydrogen phosphate; the modified sepiolite fibers The parts by weight of each raw material are respectively 15-30 parts of sepiolite, 1-8 parts of N,N-dimethylformamide and 2-10 parts of flame retardant polymer; The parts by weight of raw materials are 30-45 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphorus spiro[5.5]undecane, 3-8 parts of antioxidant and Dimethyl sulfoxide 15‑30 parts; by hot pressing two layers of heat insulation materials together, the heat insulation performance of the heat insulation material is improved, the thermal conductivity of the heat insulation material is effectively reduced, and the prepared heat insulation is also improved The compressive strength and tensile strength of the material also have the special performance of reflecting energy very well.

Description

technical field [0001] The invention relates to the technical field of heat insulation materials, in particular to a fiber-reinforced composite heat insulation material and a preparation method thereof. Background technique [0002] Thermal insulation materials are widely used in metallurgy, non-ferrous metals, machinery, petrochemical, electric power and other fields. The heat insulation material has the characteristics of low density, high flexibility, waterproof, etc., can collect excess heat, has good randomness, has no cavity, and can avoid tearing and falling off under negative wind pressure. Thermal insulation materials are generally divided into inorganic and organic. Organic insulation materials mainly include polyurethane foam, polystyrene board, phenolic foam, etc. Inorganic heat insulation materials are mainly concentrated in materials with certain heat insulation effects such as airgel felt, glass wool, rock wool, expanded perlite, and micro-nano heat insulati...

Claims

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Application Information

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Patent Type & AuthorityPatents(China)
IPC IPC(8): C04B28/00C03C13/06C04B20/02
CPCC03C13/06C04B20/023C04B28/005C04B2201/32C04B2201/50C04B14/064C04B14/4656C04B14/4681C04B16/0616C04B14/4643C04B14/4625C04B22/16
Inventor张宗军赵宝军孟庆飞其他发明人请求不公开姓名
OwnerGUANGDONG HAILONG CONSTR TECH CO LTD