A kind of fiber-reinforced composite thermal insulation material and preparation method thereof
A fiber-reinforced composite and thermal insulation material technology, applied in the field of thermal insulation materials, can solve the problems that thermal insulation materials do not have reflective energy and oxidation resistance, cannot meet the design and use requirements, and the heat resistance of materials is difficult to solve, and achieve good results. Antioxidant effect, no decline in mechanical properties, and improved compatibility
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Embodiment 1
[0031] A fiber-reinforced composite thermal insulation material, the raw materials are 30 parts by weight of silica airgel powder, 15 parts of aluminum silicate fiber, 10 parts of aluminum solution, 5 parts of potassium hexatitanate whisker, electrospun poly 8 parts of vinylidene fluoride micro-nano fiber, 45 parts of modified sepiolite fiber, 35 parts of modified nano-alumina fiber and 1 part of aluminum dihydrogen phosphate;
[0032] The parts by weight of each raw material in the modified sepiolite fiber are 15 parts of sepiolite, 40 parts of hydrochloric acid, 3 parts of toluene, 1 part of N,N-dimethylformamide and 2 parts of flame retardant polymer;
[0033]The parts by weight of each raw material in the flame retardant polymer are 30 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 13 parts of amine, 5 parts of magnesium hydroxide, 1 part of dispersant, 3 parts of antioxidant and 15 parts of dimethyl sulfoxide;
[0034] The preparatio...
Embodiment 2
[0047] A fiber-reinforced composite thermal insulation material, the raw materials are 50 parts by weight of silica airgel powder, 35 parts of aluminum silicate fiber, 15 parts of aluminum solution, 8 parts of potassium hexatitanate whisker, electrospun poly 12 parts of vinylidene fluoride micro-nano fiber, 58 parts of modified sepiolite fiber, 39 parts of modified nano-alumina fiber and 6 parts of aluminum dihydrogen phosphate;
[0048] The parts by weight of each raw material in the modified sepiolite fiber are 23 parts of sepiolite, 60 parts of hydrochloric acid, 5 parts of toluene, 6 parts of N,N-dimethylformamide and 7 parts of flame retardant polymer;
[0049] The parts by weight of each raw material in the flame retardant polymer are 40 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 20 parts of amine, 8 parts of magnesium hydroxide, 1-6 parts of dispersant, 5 parts of antioxidant and 25 parts of dimethyl sulfoxide;
[0050] The pre...
Embodiment 3
[0063] A fiber-reinforced composite thermal insulation material, the raw materials are 75 parts by weight of silica airgel powder, 60 parts of aluminum silicate fiber, 20 parts of aluminum solution, 10 parts of potassium hexatitanate whisker, electrospun poly 15 parts of vinylidene fluoride micro-nano fiber, 65 parts of modified sepiolite fiber, 45 parts of modified nano-alumina fiber and 9 parts of aluminum dihydrogen phosphate;
[0064] The parts by weight of each raw material in the modified sepiolite fiber are 30 parts of sepiolite, 75 parts of hydrochloric acid, 7 parts of toluene, 8 parts of N,N-dimethylformamide and 10 parts of flame retardant polymer;
[0065] The parts by weight of each raw material in the flame retardant polymer are 45 parts of 3,9-dichloro-2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane, ethylene di 25 parts of amine, 10 parts of magnesium hydroxide, 1-6 parts of dispersant, 8 parts of antioxidant and 30 parts of dimethyl sulfoxide;
[0066] The ...
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