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Maillard Reaction Tobacco Flavor of Maple Maple Extract, Preparation Method and Application in Heat-Not-Burn Cigarettes

A Maillard reaction and heat-not-burn technology, applied in the field of tobacco flavors, can solve the problems of limited smoking quality and aroma richness, low content of volatile aroma components, and limited application of heat-not-burn cigarettes, and achieve enhanced and improved aroma characteristics, high aroma intensity, and shortened reaction time

Active Publication Date: 2022-03-25
CHINA TOBACCO HENAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the content of volatile aroma components in maple extract is low, and its main components are non-volatile components such as sucrose, maltose, fructose and glucose. The effect of improving the smoking quality and aroma richness of heat-not-burn cigarettes is limited, which greatly limits its application in heat-not-burn cigarettes

Method used

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  • Maillard Reaction Tobacco Flavor of Maple Maple Extract, Preparation Method and Application in Heat-Not-Burn Cigarettes
  • Maillard Reaction Tobacco Flavor of Maple Maple Extract, Preparation Method and Application in Heat-Not-Burn Cigarettes

Examples

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Effect test

Embodiment 1

[0023] A preparation method of Maple maple extract Maillard reaction tobacco flavor, which comprises the following steps:

[0024] 1) Dissolving: add water with 1 times the mass of maple extract to 50.00 g maple extract, stir and mix evenly to obtain maple extract solution;

[0025] 2) Acid hydrolysis: Add citric acid (the amount of citric acid is about 1.4% of the mass of the maple maple extract solution) to the maple maple extract solution to adjust the pH value to 1-2, and then stir and react at 85 °C for 2.5 h, obtain maple maple extract hydrolyzate;

[0026] 3) Microwave reaction: add proline with a mass of 1.0‰ of maple maple extract to the hydrolyzed solution of maple maple extract, after mixing evenly, adjust the pH to 8 with potassium hydroxide aqueous solution with a concentration of 2 mol / L, and then place it in a microwave oven 500W microwave reaction for 5min to carry out Maillard reaction. After the reaction is finished, it is naturally cooled to room temperatu...

Embodiment 2

[0028] A preparation method of Maple maple extract Maillard reaction tobacco flavor, which comprises the following steps:

[0029] 1) Dissolving: Add 10% (v / v) propylene glycol-water solution with 3 times the mass of maple extract to 50.00 g maple extract, stir and mix well to obtain maple extract solution;

[0030] 2) Acid hydrolysis: Add malic acid (the amount of malic acid is about 1.8% of the mass of the maple maple extract solution) to the maple maple extract solution to adjust the pH value to 1-2, and then stir and react at 100 °C for 1.5 h, obtain maple maple extract hydrolyzate;

[0031] 3) Microwave reaction: Alanine with a mass of 0.5‰ of Maple maple extract was added to the hydrolyzed solution of maple maple extract. After mixing evenly, the pH was adjusted to 9 with an aqueous solution of potassium hydroxide with a concentration of 1 mol / L, and then placed in a microwave oven. In 400W microwave reaction for 7min to carry out Maillard reaction. After the reaction ...

Embodiment 3

[0033] A preparation method of Maple maple extract Maillard reaction tobacco flavor, which comprises the following steps:

[0034] 1) Dissolution: add 50% (v / v) propylene glycol-water solution with 5 times the mass of the maple extract to 50.00 g of maple extract, stir and mix evenly to obtain a maple extract solution;

[0035] 2) Acid hydrolysis: add tartaric acid (the amount of tartaric acid is about 1.1% of the mass of the maple maple extract solution) to the maple maple extract solution to adjust the pH value to 1-2, and then stir and react at 70 ° C for 5 hours, Obtain maple maple extract hydrolyzate;

[0036] 3) Microwave reaction: Add serine with a mass of 5.0‰ of Maple maple extract to the hydrolyzed solution of maple maple extract. After mixing evenly, adjust the pH to 10 with potassium hydroxide aqueous solution with a concentration of 1 mol / L, and then place it in a microwave oven for 600W microwave reaction for 4min to carry out Maillard reaction. After the react...

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Abstract

The invention relates to a method for preparing a maple extract extract Maillard reaction cigarette spice, which comprises the following steps: 1) dissolving: uniformly mixing the maple extract extract with a solvent to obtain a maple extract extract solution; 2) acid hydrolysis : Adjust the pH of the maple extract solution to 1-2, and then react at 70-105°C for 1-5 hours to obtain the hydrolyzate of maple extract; 3) Microwave reaction: add amino acids to the hydrolyzate of maple extract , after mixing, adjust the pH to 8-11, then react in microwave at 300-700W for 2-10 min, and cool naturally after the reaction to obtain the maple maple extract Maillard reaction tobacco flavor. The tobacco flavor not only maintains the style and product characteristics of the maple extract itself, but also overcomes the application limitations of the maple extract in heat-not-burn cigarettes, making maple extract available in heat-not-burn cigarettes. better application.

Description

technical field [0001] The invention belongs to the technical field of tobacco flavors, and in particular relates to a Maillard reaction tobacco flavor of Maple maple extract, a preparation method thereof and an application in heat-not-burn cigarettes. Background technique [0002] Heat-not-burn cigarettes are a new type of tobacco products. They use a special heat source to heat a cigarette heating rod made of tobacco material, and volatilize nicotine and aroma substances in a non-combustion state, thereby producing nicotine for consumers to inhale. smoke. Compared with traditional cigarettes, because the heating temperature of heat-not-burn cigarettes is relatively low, the amount of tar and harmful components released is low, and no sidestream smoke is generated, which has little impact on non-smokers. Therefore, with the global tobacco control environment. Under the background of the increasingly severe situation and consumers' increasing concern for health, heat-not-bu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00A24B15/30A24B3/12
CPCA24B3/12A24B15/306C11B9/0003
Inventor 蔡莉莉王宏伟张俊岭刘前进赵志伟李小福王东席高磊陈芝飞刘文博胡少东孙志涛宋金勇邱建华
Owner CHINA TOBACCO HENAN IND