A kind of anti-temperature and anti-salt extreme pressure lubricant for high-density drilling fluid and preparation method thereof
A technology of extreme pressure lubricants and drilling fluids, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems that do not involve temperature resistance and adhesion coefficient reduction, and achieve excellent temperature and salt resistance, Reduced friction coefficient and strong hydrolytic stability
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Embodiment 1
[0040] While stirring, add 80 parts of sulfonated methyl oleate into the reaction kettle, heat up to 50 °C, add 6 parts of oleic acid and stir for 30 min, then heat up to 95 °C, then add 6 parts of sulfurized fatty acid methyl ester and 2 One part of methylene bis-dibutyl dithiocarbamate was stirred for 20 min, and finally 3 parts of emulsifier were added (the emulsifier was a mixture of nonionic surfactants OP-10 and SP-80, and the mass mixing ratio was OP- 10: SP-80=2:3) and 3 parts of silicone defoamer cooled to room temperature while stirring, the resulting black red liquid is non-fluorescence anti-temperature and anti-salt extreme pressure lubricant for high-density drilling fluid.
Embodiment 2
[0042] While stirring, add 82 parts of sulfonated methyl oleate into the reaction kettle, heat up to 60 °C, add 5 parts of oleic acid and stir for 30 min, then heat up to 100 °C, then add 5 parts of sulfurized fatty acid methyl ester and 3 One part of methylene bis-dibutyl dithiocarbamate was stirred for 20 min, and finally 3 parts of emulsifier were added (the emulsifier was a mixture of nonionic surfactants OP-10 and SP-80, and the mass mixing ratio was OP- 10: SP-80=2:3) and 2 parts of silicone defoamer cooled to room temperature while stirring, the resulting black-red liquid is non-fluorescence anti-temperature and anti-salt extreme pressure lubricant for high-density drilling fluid.
Embodiment 3
[0044] While stirring, add 82 parts of sulfonated methyl oleate into the reaction kettle, heat up to 95 °C, add 5 parts of oleic acid and stir for 30 min, then heat up to 100 °C, add 5 parts of sulfurized fatty acid methyl ester and 3 parts Methylene bis-dibutyl dithiocarbamate was stirred for 20 min, and 3 parts of emulsifier were added (the emulsifier was a mixture of nonionic surfactants OP-10 and SP-80, and the mass mixing ratio was OP-10: SP-80=2:3) and 2 parts of silicone defoamer cooled to room temperature while stirring, the resulting black red liquid is non-fluorescent anti-temperature and anti-salt extreme pressure lubricant for high-density drilling fluid.
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