A kind of nanocrystalline alloy magnetic core and preparation method thereof
A nanocrystalline alloy, magnetic core technology, applied in the direction of transformer/inductor core, inductor/transformer/magnet manufacturing, magnetic objects, etc. The problem of low relaxation frequency of alloy materials can achieve the effect of broadening the product market and application prospects, reducing high-frequency loss, and improving grain nucleation density and dispersion.
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Embodiment 1
[0064] This implementation provides a high relaxation frequency nanocrystalline magnetic core for a high frequency transformer. The preparation method of the magnetic core is as follows.
[0065] (1) First, the alloy composition selects Fe 76 Si 13 B 8 Nb 2 Cu 1 , using rapid cooling technology to prepare quenched alloy strips, the specific steps are: Fe, Si, B, Cu and Nb of industrial raw materials are batched according to the components of this embodiment; raw materials with a good ratio are put into an induction melting furnace In the aluminum crucible inside, high temperature melting and heat preservation for 15 minutes, then the melted mixture is poured into a copper mold and cooled to prepare a master alloy steel ingot with uniform composition. The roll speed was 30 m / s). Denoted as the quenched alloy strip M1, the thickness of the quenched alloy strip M1 is 20 microns.
[0066] Carry out XRD test to this as-quenched alloy strip M1, detect its microstructure, the ...
Embodiment 2
[0078] This implementation provides a high relaxation frequency nanocrystalline magnetic core for a high frequency transformer. The preparation method of the magnetic core is as follows.
[0079] (1) First, the alloy composition selects Fe 75.5 Si 13 B 8 Nb 2 Cu 1 (VCAl) 0.5 , using rapid cooling technology to prepare quenched alloy strip, the specific steps are basically the same as in Example 1, the difference is that the copper roll speed is 35m / s. Denoted as quenched alloy strip M2. The as-quenched alloy strip M2 has a strip thickness of 18 microns.
[0080] Carry out XRD test to this quenched alloy strip M2, observe its microstructure, the result is as follows Figure 12 shown. The XRD pattern of the free surface and the rolled surface of the as-quenched alloy strip M2 shows that it has a broadened diffuse diffraction peak at 45°; indicating that the microstructure of all regions of the as-quenched strip is completely amorphous .
[0081] (2) Then, enclose and ...
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