Pesticide composition and preparation method thereof
A technology of pesticide composition and liquid medicine, which is applied in the field of pesticides, can solve the problems of many impurities, low extraction yield, low purity, etc., and achieve the effects of high penetration efficiency, good slow-release effect, and excellent antioxidant property
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Embodiment 1
[0070] Preparation of toosendanin solution
[0071] refer to figure 1 Shown, the preparation method of toosendanin solution in the present embodiment may further comprise the steps:
[0072] S1. Take 1 kg of Toosendan powder and 10L of 75% alcohol, put it into an ultrasonic extraction pot for extraction, separate the alcohol liquid after the extraction is completed, filter the liquid, and separate the solid and liquid to obtain the alcohol liquid;
[0073] Among them, the extraction time is 1 hour, the wavelength / frequency of ultrasonic waves is 28Hz, the power is 1500w, and the cooling water temperature is 28°C;
[0074] S2. Concentrate the alcohol liquid obtained in step S1 in a vacuum, then add it into an aqueous solution, pour the aqueous solution into petroleum ether at a ratio of 1:1 to obtain a mixed solution a, then pour the mixed solution a into a stirring bottle, and perform mechanical stirring , stirred for 25 to 30 minutes, poured the stirred mixed solution a int...
Embodiment 2
[0119] Extraction of croton oil
[0120]The preparation method of croton oil in the present embodiment comprises the following steps: take by weighing 1000g croton powder and 8000mL sherwood oil, put into ultrasonic extraction pot, extraction time is 1 hour, the wavelength of ultrasonic wave is 28Hz, and power is 1500w, and cooling water water temperature is At 28°C, after the extraction is complete, separate the solid from the liquid, and precipitate the solution for 12 hours, then filter through a 120 μm micropore to obtain a petroleum ether clear liquid, and then put the obtained petroleum ether clear liquid into a rotary evaporator to concentrate to obtain 460 mL of croton oil.
[0121] Wherein, the content of crotonoleic acid in the obtained croton oil in the present embodiment is 2.3%.
Embodiment 3
[0123] Configure 1000mL of pesticide composition
[0124] The pesticide composition of configuring 1000mL in the present embodiment comprises the following steps:
[0125] a, take by weighing toosendanin solution 1000mL prepared in embodiment 1, croton oil 35mL prepared in embodiment 2, 25mL limonene, 95mL silicone surfactant SilwetL 77, 4mL vegetable oil emulsifier;
[0126] b. Add the toosendanin solution, croton oil, and limonene stock solution weighed in b into the emulsifier in turn, slowly add silicone surfactant and vegetable oil emulsifier during the emulsification process, and stir and emulsify for 15 to 20 minutes to obtain 1000mL of pesticide composition.
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