A kind of tobacco extract and preparation method thereof

A technology of tobacco extract and tobacco, which is applied in the field of tobacco, can solve the problems of difficulty in dissolving and uniformity, and achieve good application prospects, reduce content, and the effect of tobacco's original fragrance and mellowness

Active Publication Date: 2022-04-22
CHINA TOBACCO FUJIAN IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] (2) Use a specific solvent to extract the enzyme-treated product in a targeted manner, and extract the tobacco aroma components that can be dissolved in glycerin and propylene glycol, so as to solve the problem that the general tobacco extract is difficult to dissolve evenly in the e-cigarette liquid of the propylene glycol and glycerin solvent system The problem;

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] Weigh 1 g of pectin lyase and 1 g of cellulase, and mix them to prepare an enzyme treatment solution. Add 20g of water, stir evenly, add 0.1g of acetic acid to adjust the pH to 5.5. Use a compressed air spray pump to evenly spray the enzyme treatment solution on 1 kg of leaf group tobacco leaves, and seal it with a plastic bag. The sealed material was subjected to enzyme treatment in a thermostat at 45° C. for 8 hours.

[0063] Weigh 2kg of propylene glycol, 1kg of glycerin, 5kg of ethanol, and 2kg of water, add them to an ultrasonic extractor, and stir evenly. Add the enzyme-treated tobacco leaves into an ultrasonic extractor and soak for 3 hours. Turn on the ultrasonic wave and extract for 40 minutes. Extraction conditions: ultrasonic frequency 25KHz, ultrasonic power 1KW, temperature 45°C. Open the valve, release the extract, and filter with filter paper to obtain 9.5kg of extract clear liquid.

[0064] Concentrate the extracted clear liquid, concentrate it unde...

experiment example 2

[0067] Weigh 0.8g of pectin lyase and 1.2g of cellulase, and mix them to prepare an enzyme treatment liquid. Add 20g of water, stir evenly, add 0.12g of acetic acid to adjust the pH to 5.0. Use a compressed air spray pump to evenly spray the enzyme treatment solution on 1 kg of leaf group tobacco leaves, and seal it with a plastic bag. The seals were incubated in an incubator at 45°C for 6 hours.

[0068] Weigh 2kg of propylene glycol, 1kg of glycerin, 5kg of ethanol, and 2kg of water, add them to an ultrasonic extractor, and stir evenly. Add the enzyme-treated tobacco leaves into an ultrasonic extractor and soak for 3 hours. Turn on the ultrasonic wave and extract for 50 minutes. Extraction conditions: ultrasonic frequency 25KHz, ultrasonic power 1KW, temperature 45°C. Open the valve, release the extract, and filter with filter paper to obtain 9.65kg of extract clear liquid.

[0069] Concentrate the extracted clear liquid, concentrate under vacuum negative pressure (-0.0...

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PUM

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Abstract

The invention relates to a preparation method of tobacco extract, comprising the following steps: 1) using pectin lyase and cellulase to enzymatically treat tobacco; 2) mixing the product of step 1) with a solvent, performing ultrasonic extraction, and then Separate the supernatant from the product; wherein, the solvent contains 15-25% propylene glycol, 5-15% glycerin, 40-60% ethanol, and 15-25% water; 3) Concentrate the supernatant in step 2) under reduced pressure , concentrated until no solvent is distilled off to obtain a concentrate; 4) mix the concentrate with propylene glycol at a weight ratio of 1:1 to 5 to obtain a mixture, carry out molecular distillation on the mixture, and collect the distilled light components. The tobacco extract is used in e-cigarette liquid with improved sensory quality.

Description

technical field [0001] The invention belongs to the field of tobacco, and in particular relates to a tobacco extract and a preparation method thereof. Background technique [0002] With the increasing emphasis on smoking and health issues and the continuous strengthening of tobacco control efforts, the development environment of tobacco products has undergone major and profound changes. New tobacco products such as e-cigarettes and heat-not-burn cigarettes have developed rapidly due to their low harm and environmental impact. According to statistics, in 2017, the global new tobacco product market size was about 17.1 billion US dollars, a year-on-year increase of 38.7%. [0003] In the prior art, the e-cigarette liquid used for smoking e-cigarettes mainly uses propylene glycol and glycerin as solvents. Traditional cigarette tobacco extract aroma raw materials have problems such as low miscibility, sugar and macromolecular impurities, and easy burnt when applied to e-cigaret...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/24A24B15/30A24B15/167
CPCA24B15/24A24B15/30A24B15/167
Inventor 方钲中陈辉赖炜扬杨斌操晓亮连芬燕林德洪赵世兴黄艳
Owner CHINA TOBACCO FUJIAN IND
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