Electrolyte solution, calcium ion secondary battery and preparation method thereof
A secondary battery, electrolyte technology, applied in secondary batteries, electrolytes, circuits, etc., can solve the problems of restricting the development and application of calcium ion secondary batteries, poor ionic conductivity, serious self-discharge phenomenon, etc., to reduce solvation. effect, low cost, simple material effect
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[0054] As an optional embodiment of the present invention, the calcium salt includes calcium hexafluorophosphate, calcium tetrafluoroborate, calcium chloride, calcium carbonate, calcium sulfate, calcium nitrate, calcium fluoride, calcium trifluoromethanesulfonate, bis( Any one or a combination of at least two of calcium trifluoromethylsulfonyl)imide, calcium bisfluorosulfonyl imide, or calcium perchlorate, preferably calcium hexafluorophosphate and / or calcium tetrafluoroborate.
[0055] As an optional embodiment of the present invention, the lithium salt includes any one of lithium hexafluorophosphate, lithium tetrafluoroborate, lithium bis(trifluoromethylsulfonyl)imide, lithium perchlorate or lithium trifluoromethanesulfonate Or a combination of at least two, preferably lithium hexafluorophosphate and / or lithium tetrafluoroborate;
[0056] And / or, the sodium salt includes any one or a combination of at least two of sodium hexafluorophosphate, sodium perchlorate, sodium nitrat...
Embodiment 1
[0105] This embodiment is a calcium ion secondary battery, including a negative electrode, a separator, an electrolyte and a positive electrode.
[0106] Wherein, the electrolytic solution includes calcium salt and lithium salt, the calcium salt is calcium hexafluorophosphate, and the lithium salt is lithium hexafluorophosphate.
[0107] The specific material composition and preparation method of the calcium ion secondary battery provided in this embodiment are as follows:
[0108] (a) Preparation of positive electrode: Add 0.8g expanded graphite, 0.1g conductive carbon black, and 0.1g polyvinylidene fluoride to 2mL nitrogen methyl pyrrolidone solution, grind thoroughly to obtain a uniform slurry; then evenly coat the slurry on aluminum foil The surface (i.e. the positive electrode current collector) is vacuum-dried, and the dried electrode sheet is cut into a disc with a diameter of 10mm, and it is used as the positive electrode after compaction (10MPa, 10s);
[0109] (b) Pr...
Embodiment 2
[0114] This embodiment provides a calcium ion secondary battery. The mass of calcium hexafluorophosphate in the electrolyte is adjusted to 0.66 g, and the rest of the composition and preparation method are the same as those in Embodiment 1.
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