A method for preparing bi nanosheets by electrochemical exfoliation
A technology of nanosheet and exfoliation method, which is applied in chemical instruments and methods, catalyst activation/preparation, nanotechnology, etc., can solve the problems of low melting point of metal bismuth and difficulty in realizing metal bismuth, and achieve high purity, good industrialization prospects, and surface The effect of more active sites
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Embodiment 1
[0040](1) Add 50mL of 0.5mol·L to the cathode and anode electrolytic cells of H-Cell (100mL specification) -1 NaI solution, and pass 20min N into the cathode electrolytic cell 2 ;
[0041] (2) Take the size as 5mm 3 , 99.99% pure metal Bi block is used as cathode, Pt sheet electrode is used as anode, DC regulated power supply provides 15V voltage, and N is continuously passed to the cathode electrolytic cell during power-on. 2 ;
[0042] (3) After energizing for 2 hours, the solution in the cathodic electrolytic cell was vacuum filtered by a vacuum filter, the precipitate was fully washed with ultrapure water, and the product was collected and dried in an electric vacuum oven at 80°C for 4 hours to obtain Bi nanosheets.
[0043] Characterization tests:
[0044] Carry out XRD test to the Bi nanosheet prepared in this embodiment, figure 1 For the XRD spectrum of the Bi nanosheets prepared in this example, the PDF card comparison proves that the prepared product is Bi. At th...
Embodiment 2
[0047] (1) Add 50mL of 1.0mol L to the cathode and anode electrolytic cells of H-Cell (100mL specification) -1 NaI solution, and pass 20min N into the cathode electrolytic cell 2 ;
[0048] (2) Take the size as 5mm 3 , 99.99% pure metal Bi block is used as cathode, Pt sheet electrode is used as anode, DC regulated power supply provides 30V voltage, and N is continuously passed to cathode electrolytic cell during power-on process 2 ;
[0049] (3) After energizing for 3 hours, the solution in the cathodic electrolytic cell was vacuum filtered by a vacuum filter, the precipitate was fully washed with ultrapure water, and the product was collected and dried in an electric vacuum oven at 60°C for 6 hours to obtain Bi nanosheets.
Embodiment 3
[0051] (1) Add 50mL of 0.7mol·L to the cathode and anode electrolytic cells of H-Cell (100mL specification) -1 NaI solution, and pass 20min N into the cathode electrolytic cell 2 ;
[0052] (2) Take the size as 5mm 3 , 99.99% pure metal Bi block is used as cathode, Pt sheet electrode is used as anode, DC regulated power supply provides 10V voltage, and N is continuously passed to the cathode electrolytic cell during power-on process 2 ;
[0053] (3) After electrifying for 4 hours, the solution in the cathodic electrolytic cell was vacuum filtered by a vacuum filter, the precipitate was fully washed with ultrapure water, and the product was collected and dried in an electric vacuum oven at 70°C for 5 hours to obtain Bi nanosheets.
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