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Sintered synthetic slag and preparation method of sintered synthetic slag

A technology for synthesizing slag and mixed liquid, which is applied in the field of iron and steel smelting, and can solve problems such as slow melting, large dust, and easy breakage

Active Publication Date: 2020-10-30
芜湖县天海耐火炉料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Mixed-type synthetic slag is made by mixing various block and powder raw materials according to the proportion and weighing. During transportation and storage, it is very easy to be broken, damp and pulverized, so there is a lot of dust and material loss during use. , slow melting, and serious environmental pollution; pressed molding synthetic slag uses a high-pressure molding machine and is directly pressed into balls without adding a binder. Pulverization problem, and the investment cost of high pressure molding machine is relatively large
[0003] The Chinese invention patent publication number is CN1377977, which discloses a synthetic slag suitable for deoxidation and sulfur in steelmaking and its manufacturing method. The composition of the synthetic slag is: aluminum 2-15%, cerium 3-15%, magnesium 5- 8%, barium 2-10%, calcium oxide 20-50%, aluminum oxide 0-48%, magnesium oxide 2-10%, sodium silicate 2-10%, cellulose 2-8%. The production method is to mix limestone , fluorite and other high-alkalinity materials and fluxes are melted into slag, released and cooled to room temperature. The characteristic is that the slag, aluminum metallurgical slag, and calcium oxide raw materials are all broken into powders with a particle size of less than 0.5mm. Mix according to the ratio of [(2-4):(2-6):(1-3)] and add sodium silicate and cellulose at the same time, after mixing evenly, form φ10-20mm spherical synthetic slag and dry it at low temperature; the synthetic The production process of slag is cumbersome, and the cost of raw materials and preparation is relatively high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A sintered synthetic slag, comprising the following raw materials in weight percentage: 10% high-adsorption filler, 25% CaO, 10% SiO 2 , 8% MgO, 6-10% FeO, 1% CaF 2 , 0.01% of P, 5% of water, 3% of aluminum and iron balls, and the balance is impurities;

[0023] The sintered synthetic slag is made by the following method:

[0024] CaO and SiO 2 Grind into powder, then add water, MgO, FeO, CaF in sequence 2 , P, high-adsorption filler, mixed uniformly and made into a spherical shape, the particle size is controlled to be 50mm, and then mixed with aluminum-iron balls and transferred to a high-temperature furnace for firing. The temperature of the high-temperature furnace is controlled at 1200 ° C, and the firing time is 3 hours. , to obtain the sintered synthetic slag.

[0025] High adsorption packing is made by the following methods:

[0026] Step (1) After calcining illite at 450°C for 1 hour, add it to a 10% sodium chloride solution by mass fraction, heat in a wat...

Embodiment 2

[0030] A sintered synthetic slag, comprising the following raw materials in weight percentage: 12% of high-adsorption filler, 28% of CaO, 12% of SiO 2 , 9% MgO, 8% FeO, 1.5% CaF 2 , 0.02% of P, 6% of water, 4% of aluminum and iron balls, and the balance is impurities;

[0031] The sintered synthetic slag is made by the following method:

[0032] CaO and SiO 2 Grind into powder, then add water, MgO, FeO, CaF in sequence 2 , P, high-adsorption filler, mixed uniformly and made into a spherical shape, the particle size is controlled to be 50mm, and then mixed with aluminum-iron balls and transferred to a high-temperature furnace for firing. The temperature of the high-temperature furnace is controlled at 1200 ° C, and the firing time is 3 hours. , to obtain the sintered synthetic slag.

[0033] High adsorption packing is made by the following methods:

[0034] Step (1) After calcining illite at 450°C for 1 hour, add it to a 10% sodium chloride solution by mass fraction, heat in...

Embodiment 3

[0038] A sintered synthetic slag, containing the following raw materials in weight percentage: 14% high-adsorption filler, 30% CaO, 18% SiO 2 , 9% MgO, 8% FeO, 2.0% CaF 2 , 0.02% of P, 6% of water, 5% of aluminum and iron balls, and the balance is impurities;

[0039] The sintered synthetic slag is made by the following method:

[0040] CaO and SiO 2 Grind into powder, then add water, MgO, FeO, CaF in sequence 2 , P, high-adsorption filler, mixed uniformly and made into a spherical shape, the particle size is controlled to be 50mm, and then mixed with aluminum-iron balls and transferred to a high-temperature furnace for firing. The temperature of the high-temperature furnace is controlled at 1200 ° C, and the firing time is 3 hours. , to obtain the sintered synthetic slag.

[0041] High adsorption packing is made by the following methods:

[0042] Step (1) After calcining illite at 450°C for 1 hour, add it to a 10% sodium chloride solution by mass fraction, heat in a wate...

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PUM

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Abstract

The invention discloses sintered synthetic slag. The sintered synthetic slag is prepared from the following raw materials of, in percentage by weight, 10%-15% of a high-adsorption filler, 25%-35% of CaO, 10%-20% of SiO2, 8%-10% of MgO, 6%-10% of FeO, 1%-2.5% of CaF2, 0.01%-0.03% of P, 5%-8% of water, 3%-5% of ferro-aluminum balls and the balance impurities. The invention further discloses a preparation method of the sintered synthetic slag. The preparation method comprises the following steps that CaO and SiO2 are ground into powder, water, MgO, FeO, CaF2, P and the high-adsorption filler aresequentially added, and after the water, MgO, FeO, CaF2, P and the high-adsorption filler are uniformly mixed, balls are made; particle size is controlled to be 50mm-60mm, then the balls are transferred into a high-temperature furnace for firing after the balls are uniformly mixed with the ferro-aluminum balls, the temperature of the high-temperature furnace is controlled to be 1200DEG C-1300 DEGC, the firing time is 3 hours, and the sintered synthetic slag is prepared; the high-adsorption filler can remove hydrogen and floating oxidation slag inclusion inside the molten steel, so that the molten steel is purer, the slag inclusion is adsorbed by the high-adsorption filler with high adsorption performance, the slag inclusion escapes from a melt rapidly, and the purity of the molten steel is improved.

Description

technical field [0001] The invention belongs to the technical field of iron and steel smelting, in particular to a sintered synthetic slag and a preparation method thereof. Background technique [0002] Synthetic slag refining technology has become an important process in the production of clean steel in the steelmaking process. Because synthetic slag refining technology can reduce the content of oxygen, sulfur and inclusions in steel, it is widely used. In steelmaking production using synthetic slag refining technology, synthetic slag is usually divided into mixed synthetic slag, pressed synthetic slag and pre-melted synthetic slag. Mixed-type synthetic slag is made by mixing various block and powder raw materials according to the proportion and weighing. During transportation and storage, it is very easy to be broken, damp and pulverized, so there is a lot of dust and material loss during use. , slow melting, and serious environmental pollution; pressed molding synthetic...

Claims

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Application Information

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IPC IPC(8): C21C7/076
CPCC21C7/076Y02P10/20
Inventor 吴大宏童振兰
Owner 芜湖县天海耐火炉料有限公司
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