Preparation method of graphene cigarette smoke filter screen and obtained filter screen
A graphene and filter technology, which is applied in the direction of e-liquid filter elements, separation methods, and dispersed particle filtration, can solve the problems of limited filtering effect, unsatisfactory adsorption effect of harmful gases, and unsatisfactory adsorption effect, and achieve broad application prospects Effect
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Embodiment 1
[0029] A kind of graphene cigarette smoke filter screen, its preparation method comprises the following steps:
[0030] (1) Disperse 1g of graphene oxide in 10g of water to form a graphene oxide solution, add 2g of calcium chloride and 0.5g of sodium carbonate to the graphene oxide solution, mix and react, then add 0.42mL of ethanol, 0.2g of ammonia and 0.33 g ethylenediamine, reacted at 90°C for 6h, then added 50g of hydrochloric acid with a mass fraction of water of 10%, filtered, washed, and dried to obtain porous graphene;
[0031] (2) Take 100 mL of aqueous sodium hydroxide solution with a concentration of 2 mol / L, add 0.4 mol of terephthalic acid, stir well, then add 0.2 mol of nickel nitrate, react at 50 ° C for 5 h, filter, and dry to obtain a nickel metal organic framework solution ;
[0032] (3) get activated carbon, the porous graphene that step (1) obtains, the nickel metal organic framework solution that step (2) obtains, described activated carbon: porous graphe...
Embodiment 2
[0035] A kind of graphene cigarette smoke filter screen, its preparation method comprises the following steps:
[0036] (1) Disperse 1g of graphene oxide in 20g of water to form a graphene oxide solution, add 5g of calcium chloride and 0.2g of sodium carbonate to the graphene oxide solution, mix and react, then add 0.25mL of ethanol, 0.1g of ammonia and 0.2 g ethylenediamine, reacted at 100°C for 5h, then added 100g of hydrochloric acid with a mass fraction of water of 15%, filtered, washed, and dried to obtain porous graphene;
[0037] (2) Take 100 mL of aqueous sodium hydroxide solution with a concentration of 5 mol / L, add 1 mol of terephthalic acid, stir evenly, then add 0.5 mol of nickel nitrate, react at 100 ° C for 4 hours, filter, and dry to obtain a nickel metal organic framework solution;
[0038] (3) get activated carbon, the porous graphene that step (1) obtains, the nickel metal organic framework solution that step (2) obtains, described activated carbon: porous gr...
Embodiment 3
[0041] A graphene cigarette smoke filter, its preparation method comprises the following steps:
[0042](1) Disperse 1g of graphene oxide in 15g of water to form a graphene oxide solution, add 3g of calcium chloride and 0.25g of sodium carbonate to the graphene oxide solution, mix and react, then add 0.25mL of ethanol, 0.1g of ammonia and 0.2 g ethylenediamine, reacted at 100°C for 5h, then added 100g of hydrochloric acid with a mass fraction of water of 15%, filtered, washed, and dried to obtain porous graphene;
[0043] (2) Take 100 mL of aqueous sodium hydroxide solution with a concentration of 3 mol / L, add 0.6 mol of terephthalic acid, stir well, then add 0.3 mol of nickel nitrate, react at 100 ° C for 4 hours, filter, and dry to obtain a nickel metal organic framework solution ;
[0044] (3) get activated carbon, the porous graphene that step (1) obtains, the nickel metal organic framework solution that step (2) obtains, described activated carbon: porous graphene: the m...
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