Production method for glyceryl ether-containing composition, and glyceryl ether-containing composition
A manufacturing method and technology for glycerol ethers, which are applied in the field of the manufacture of glycerol ether-containing compositions and the fields of glycerol ether-containing compositions, can solve the problems of limited use concentration range, increased demand for cosmetic materials, low safety and the like, and can prevent oxidation The effect of deterioration and maintenance of quality
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Synthetic example 1
[0065] By reacting 3.0 g of hexanol and 2.1 g of epichlorohydrin at 80° C. for 4 hours to obtain hexyl glycidyl ether as an intermediate, hydrolyzing the obtained hexyl glycidyl ether to obtain monohexyl glycidyl ether containing The product 2.7g.
Synthetic example 2
[0067] After obtaining cyclohexyl glycidyl ether as an intermediate by reacting 3.2 g of cyclohexanol and 2.1 g of epichlorohydrin at 80° C. for 4 hours, hydrolyzing the obtained cyclohexyl glycidyl ether to obtain The product of cyclohexyl glyceryl ether 2.7g.
[0068]
[0069] 2.7 g of the monohexylglyceryl ether-containing product and the monocyclohexylglyceryl ether-containing product produced in Synthesis Example 1 and Synthesis Example 2 were respectively taken into a flask, and the pressure was reduced by a vacuum pump to the glyceryl ether-containing product. 100 parts by mass of water vapor at a flow rate of 3 parts by mass / h was added, and the deodorization treatment was carried out by contacting water vapor at 110°C and 4kPa for the time indicated in Table 1 or Table 2, respectively. Deodorizing treatment. It should be noted that the treatment time of 0 minutes means that deodorization treatment is not performed.
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