Nicotine salt and preparation method thereof

A technology of nicotine salt and nicotine, which is applied in the direction of mixing methods, chemical instruments and methods, and dissolution, can solve the problems of reducing the comfort of electronic cigarette oil atomization, affecting the smoking effect of flavors in e-liquid, and reducing e-liquid, etc. Achieve the effects of improving taste and flavor, relieving nausea and retching, and masking odor

Inactive Publication Date: 2021-06-15
SHENZHEN HUAJIA BIOLOGICAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, in order to make the physiological satisfaction of nicotine salt and the demand for taste buds match that of nicotine e-liquid, a higher concentration of nicotine salt is required in e-liquid (the concentration of nicotine salt in e-liquid needs to be as high as 40-50mg/mL ); however, h...

Method used

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  • Nicotine salt and preparation method thereof
  • Nicotine salt and preparation method thereof
  • Nicotine salt and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039]A nicotine salt, made from raw materials containing the following parts by weight: 30 parts of nicotine, 25 parts of benzoic acid, auxiliary synergist, 3 parts of erythritol, 2 parts of trehalose, and 29.8 parts of propylene glycol, totaling 100 parts; The auxiliary synergist is made of the following raw materials in parts by weight: 2 parts of propionic acid, 5 parts of levulinic acid, 0.2 part of lactic acid, 2 parts of citric acid and 1 part of tartaric acid. Among them, nicotine is artificially synthesized nicotine purchased from Henuo Biotechnology, and the model is nicotine content ≥ 99.5%.

[0040] The preparation process of the nicotine salt of the present embodiment comprises the following steps:

[0041] S1: mix the benzoic acid weighed in proportion with propylene glycol, and use a magnetic heating stirrer to heat and stir until the benzoic acid is fully dissolved;

[0042] S2: After the mixed liquid obtained in step S1 is cooled to normal temperature, mix it...

Embodiment 2 to Embodiment 9

[0086] The difference between Examples 2-9 and Example 1 is that the components or amounts of raw materials in the preparation process of nicotine salt are different, see Table 11 and Table 12 for details.

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Abstract

The invention relates to the field of electronic cigarette liquid, in particular to nicotine salt and a preparation method thereof. The nicotine salt is prepared from the following raw materials in parts by weight: 30-40 parts of nicotine, 20-25 parts of benzoic acid, 7-11 parts of auxiliary synergist and 24-43 parts of propylene glycol, in total 100 parts. The nicotine is artificially synthesized nicotine, and the EE value of levorotatory nicotine relative to dextrorotatory nicotine in the nicotine is greater than 99%. The nicotine salt can be used for preparing the electronic cigarette tobacco tar, the inhibiting effect of the high-concentration nicotine salt on perfume fragrance is reduced, the nicotine salt has the advantages of being high in throat exciting feeling, high in comfort, natural and pleasant in fragrance and free of offensive odor and peculiar smell, more pleasant and natural fragrance and taste are released, and the symptoms of nausea, vomiting, cough, excessive phlegm and the like after suction are relieved to a certain extent.

Description

technical field [0001] The present application relates to the field of electronic cigarette oil, in particular to a nicotine salt and a preparation method thereof. Background technique [0002] The common name of nicotine is nicotine, which belongs to pyridine derivative alkaloids. It has certain alkalinity and can react with acid to produce amine salt. Therefore, nicotine salt is essentially an amine salt. Mucous membrane irritation is much smaller; nicotine salt has gradually replaced traditional nicotine e-liquid because of its sensory experience similar to the physiological satisfaction of traditional cigarettes. [0003] However, in order to make the physiological satisfaction of nicotine salt and the demand for taste buds match that of nicotine e-liquid, a higher concentration of nicotine salt is required in e-liquid (the concentration of nicotine salt in e-liquid needs to be as high as 40-50mg / mL ); however, high concentrations of nicotine salts are likely to reduce ...

Claims

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Application Information

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IPC IPC(8): A24B15/167A24F40/10A24F40/40B01F3/08
CPCA24B15/167A24F40/10A24F40/40B01F23/405B01F23/43
Inventor 李智刚向寒波
Owner SHENZHEN HUAJIA BIOLOGICAL TECH
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