Methods and compositions for treating tumors
An anhydrous and injection technology, which is used in antitumor drugs, drug combinations, pharmaceutical formulations, etc.
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Embodiment 1
[0039] Embodiment 1: the preparation of aluminum sulfate for injection
[0040] As prepared by the method of reference CN100425244C. Take by weighing aluminum sulfate 800g (1.20mol) as water purifying agent, dissolve in 1090ml distilled water, filter, add 380ml concentrated sulfuric acid (containing H 2 SO 4 6.62mol), the solution was heated to 72°C, stirred and cooled in a 50°C water bath, and stirred at this temperature for 1 hour. Then the temperature was lowered to room temperature at a rate of 3-5° C. / hour, and stirring was continued for 1 hour. Suction filtration, washing with 95% ethanol three times, and drying at room temperature gave 653 g of flaky crystals with a yield of 81.6%. Weigh 600g (0.90mol) of the above-mentioned crystalline aluminum sulfate, dissolve in 1000ml distilled water, filter, add 367ml concentrated sulfuric acid (containing H 2 SO 4 6.62mol), crystallization by the same method as above. Suction filtration, washing with 95% ethanol, and dryi...
Embodiment 2
[0041] Embodiment 2: Preparation of aluminum sulfate injection
[0042] Prepared by the method of reference CN100425244C. Precisely weigh some aluminum sulfate raw materials that meet the grade for injection, 1.5g of lidocaine hydrochloride, 2mg of methylene blue, and an appropriate amount of water for injection to dissolve, add water for injection to 100ml, filter, fill in 10ml ampoules, seal, heat Autoclaved to obtain aluminum sulfate injection.
[0043] Prepare the aluminum sulfate injection of different concentration specifications according to the above-mentioned method, wherein aluminum sulfate (with anhydrous Al 2 (SO 4 ) 3 Total) contents are: 0.002%, 0.005%, 0.01%, 0.02%, 0.05%, 0.075%, 0.1%, 0.15%, 0.2%, 0.5%, 0.8%, 1%, 1.5%, 2%, 4% , 6%, 8%, and 10%, these injections can be numbered 1-18 in sequence.
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