Composition for secondary battery electrodes
A composition and electrode technology, applied in battery electrodes, secondary batteries, secondary battery manufacturing, etc., can solve the problems of electrode degradation capacity, rapid attenuation, etc.
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[0207] Preparation of 5wt% Aqueous Solution of PAI Polymer
[0208]
[0209] ODA monomer (60.0 g, 0.3 mol) was charged into a 4 neck jacketed round bottom flask equipped with an overhead mechanical stirrer. NMP (250 mL) was charged to the flask and the mixture was cooled to 10 °C under nitrogen atmosphere with gentle stirring. Equipped with a heated addition funnel, the flask was charged with TMAC (64.0 g, 0.3 moles) and heated to a minimum of 100°C. With vigorous stirring, molten TMAC was added to the solution of the diamine in NMP at a rate sufficient not to exceed 40°C. . Once the addition was complete, external heat was applied to maintain 35°C-40°C for 2 hours. Additional NMP (50 mL) was added and the reaction mixture was drained into a 500 mL beaker. The polymer solution was slowly added to water (4000 mL) in a stainless steel high shear mixer. The precipitated polymer (PAI resin) was filtered and washed multiple times with water to remove residual solvent and ...
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