Extraction method of old medicine orange spice and application of old medicine orange spice in cigarette filter tip

A technology of extracting and extracting medicines, applied in essential oils/spices, tobacco, applications, etc., which can solve the problems of unseen old medicines and spices, obstacles to the application of old medicines and spices, and difficulty in extraction, so as to facilitate scale and industrialization Production, short cycle, and the effect of improving aroma quality

Active Publication Date: 2022-08-02
CHINA TOBACCO YUNAN NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the process of extracting the spices of the old medicine orange with triacetin, it was found that there were a large number of suspended impurities in the initial extract of the old medicine orange. When the ester solution is mixed, it will form water-in-oil or oil-in-water phenomenon, which will cause severe emulsification, making it difficult to separate and extract
In the experiment, it was also found that even after the conventional filter cloth filtration method was used to remove these suspended solids, it was still difficult to extract. The main performance was that the mixture was emulsified after adding the extractant, and it was very difficult to separate the phases, resulting in the failure of the extraction. The reason was puzzling.
This technical difficulty has brought great obstacles to the application of the old medicine orange flavor in cigarette tip sticks, so there are no related reports on the application of old medicine orange flavor in cigarette tip sticks.

Method used

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  • Extraction method of old medicine orange spice and application of old medicine orange spice in cigarette filter tip
  • Extraction method of old medicine orange spice and application of old medicine orange spice in cigarette filter tip
  • Extraction method of old medicine orange spice and application of old medicine orange spice in cigarette filter tip

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A method for extracting old medicine orange spice, comprising the steps:

[0037] (1) Take 1kg of commercially available aged old medicinal oranges, add 5kg of purified water, and carry out two cell crushing ultrasonic extractions at room temperature, ultrasonic power 500W, and the first ultrasonic extraction time is 3h; the second ultrasonic extraction, extraction Time 2h; after the two extracts were combined, filtered with 500-mesh gauze, the obtained filtrate was refrigerated and settled at 4°C for 18h, and then filtered with a Buchner funnel to obtain the first extract of old medicine orange.

[0038] (2) The old medicine orange primary extract obtained in step (1) is separated by a 200-300nm microfiltration membrane module at room temperature, the solid content of the feed liquid is adjusted to 5.7%, and the microfiltration is carried out at 0.10MPa for 75min. The average flux is 17.21L / (m 2 h), collect the filtrate to obtain the old medicine orange microfiltratio...

Embodiment 2

[0047] The comparison test of membrane separation membrane concentration coupling technology and conventional separation process is carried out. The test of removal of inactive macromolecular impurities and the test of triacetin extraction effect are as follows:

[0048] When preparing Example 1 of the present invention, Comparative Example 1 and Comparative Example 2, the old medicine orange concentrate before extraction with triacetin was not added, respectively, using an AA3 continuous flow analyzer (German Bran Luebbe company) according to relevant standards: Determination refer to YC / T 216-2007 method, protein content determination refer to YC / T 249-2008 method, pectin content determination refer to YC / T 346-2010 method, cellulose content determination refer to YC / T 347-2010 method, to measure. The results are shown in the following table:

[0049] Table 1 Content comparison of macromolecular impurities in different processes

[0050]

[0051] Add 1:1 triacetin to th...

Embodiment 3

[0056] The old medicine orange flavor prepared in Example 1 is detected by gas chromatography-mass spectrometry coupled with GC-MS analysis method:

[0057] (1) Gas chromatography conditions: chromatography column: DB-5MS quartz capillary column (30m×0.25mm, 0.25μm); temperature program: the initial temperature is 60°C, maintained for 1min, and raised to 170°C at a rate of 8°C / min, Hold for 3min; rise to 260°C at a rate of 12°C / min, hold for 18min; inlet temperature: 200°C; oven temperature: 60°C; injection mode: split; column flow: 1mL / min; purge flow: 3mL / min; split ratio: 5:1; carrier gas: high-purity helium; injection volume: 1 μL; solvent delay: 2min.

[0058] (2) Mass spectrometry conditions: ionization mode: EI; electron energy: 70eV; interface temperature: 250°C; ion source temperature: 200°C; acquisition mode: scan; scanning range: 40-500amu.

[0059] (3) Qualitative analysis: By using mass spectrometry as a detector and gas chromatography, and using NIST spectral li...

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Abstract

The invention provides a method for extracting an old medicine orange spice, which comprises the following steps of: separating an old medicine orange primary extracting solution by using a microfiltration membrane and an ultrafiltration membrane to obtain an old medicine orange concentrated solution, then adding glyceryl triacetate, and carrying out ultrasonic extraction, standing, settling and layering to obtain the old medicine orange spice. The obtained old medicine orange spice has the style characteristics of unique fruity flavor, orange peel fragrance, fresh and sweet taste, sweet aftertaste and the like, in the conventional heating cigarette filter tip forming process, the obtained old medicine orange spice is added into filter tip tows, during cigarette smoking, throat stimulation can be improved, the oral cavity moist feeling, the salivation promoting feeling and the comfort feeling can be improved, and the cigarette filter tip forming effect can be improved. The effect of improving the smoking quality of the heated cigarette is achieved. The extraction method of the old medicine orange spice provided by the invention is simple in process, short in period, environment-friendly, safe, wide in application range and convenient for large-scale and industrial production, and has relatively high economic benefits.

Description

technical field [0001] The invention belongs to the technical field of tobacco flavors and fragrances, and in particular relates to an extraction method of an old medicine orange flavor and its use in a cigarette holder. Background technique [0002] Flavor and fragrance are very important to the smoking quality of cigarette products. Natural fragrance has been favored by consumers because of its ecological, safe, green, environmental protection and other advantages. In the process of shaping the aroma style of cigarettes, a variety of natural extracts are often added to solve the problems of weak aroma, poor smoke softness, weak sweetness, and insufficient thickness. [0003] Laoyaoju is one of Chaozhou cold fruits. It is a traditional medicinal cold fruit in Chaoshan area. It is the fruit of kumquat of Rutaceae family. After picking and washing, boil with water to remove the astringency. Other auxiliary materials (such as hawthorn, licorice, mint, cinnamon, etc.) are mixe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24D3/06A24D3/18
CPCC11B9/00A24D3/061A24D3/18Y02A50/30
Inventor 刘劲芸吴恒徐重军杜超王乃定蒋卓芳曹正东徐世涛刘鑫常健
Owner CHINA TOBACCO YUNAN NEW MATERIAL
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