The invention discloses a high-purity ammonia production device. The device is composed of the following components connected in sequence by pipelines: ammonia raw material tank, potassium sodium alloy tank, diaphragm compression pump, condenser, gas-liquid separation tank, and ammonia product tank. Put an activated carbon filter in the gas-liquid separation tank. In addition, the condenser and the gas-liquid separation tank are placed in the freezer. Wherein the potassium-sodium alloy tank is the core component of the present invention. Potassium-sodium alloy tanks are filled with potassium-sodium alloy - it is produced by melting high-purity metal potassium and sodium together in a certain proportion. The device can also be used in conjunction with rectification towers, distillation towers, etc. When ammonia gas passes through the potassium-sodium alloy tank, oxygen, water, carbon dioxide, carbon monoxide and other oxygen-containing gases in the gas are absorbed by the potassium-sodium alloy. In the ammonia gas passing through the device, the oxygen content, including oxygen, water, carbon dioxide, carbon monoxide, etc., is usually in the ppb (parts per billion) level, which is suitable for the production of high-purity ammonia gas.