Inspection method for Chinese medicinal composition for treating blood and qi depletion,irregular menstruation
A technology for irregular menstruation and quality detection method is applied in the field of traditional Chinese medicine compositions for treating chronic illness and physical deficiency and women with blood deficiency and qi deficiency and irregular menstruation. The effect of nourishing blood
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experiment example 1
[0023] After 150 clinical cases and 50 cases of Fukangbao oral liquid (donkey-hide gelatin, mugwort leaves, white peony root, chuanxiong, angelica, rehmannia glutinosa, licorice) were compared and observed, the report is as follows:
[0024] 1. Clinical data
[0025] The 150 cases in the treatment group were all outpatient cases, 4 cases were over 40 years old, 81 cases were 21-39 years old, 65 cases were 18-20 years old, 21 cases were 4 months old, 99 cases were 5-10 months old , 30 cases over 10 months. The 50 cases in the control group were all outpatient cases, 2 cases were over 40 years old, 30 cases were 21-39 years old, 18 cases were 18-20 years old; 7 cases were 4 months old, 30 cases were 5-10 months old , 13 cases over 10 months.
[0026] 2. Diagnostic criteria of traditional Chinese medicine: according to the "Guiding Principles of Clinical Research of New Chinese Medicines for Amenorrhea" promulgated by the Ministry of Health
[0027] (1) Diagnosis of amenorrhea...
experiment example 2
[0047] Experimental example 2 Research on Quality Control Methods
[0048] [Content Determination] is the determination method of Radix Astragali.
[0049] (1) Instruments and reagents
[0050] 1. Instruments: CS-9301PC thin-layer scanner (Shimadzu, Japan); quantitative capillary (Drummond); MettlerAE100, 200 electronic balance.
[0051] 2. Test drug: Amenorrhea No. 3 oral liquid (composition oral liquid preparation of the present invention) (produced and provided by Guangdong Yongkang Pharmaceutical Co., Ltd.; batch numbers: 020401, 020402, 020403); astragaloside IV reference substance (781-9002, China Provided by the Institute for the Control of Pharmaceutical and Biological Products); D 101 type macroporous adsorption resin (Tianjin Rubber Factory); neutral alumina for chromatography (batch number: 200321 Chemical Reagent Glass Instrument Wholesale Department of Guangzhou Pharmaceutical Company); thin-layer chromatography silica gel G (type 60) (batch number: 990313 Ch...
Embodiment 1
[0085] Example 1 oral liquid
[0086] Ejiao 216g Astragalus 180g Codonopsis 180g
[0087] Rehmannia glutinosa 120g Atractylodes macrocephala 90g Angelica 60g
[0088]For the above six flavors, take Chinese Angelica and Atractylodes Rhizoma Atractylodes Rhizome and cut them into pieces, distill them, collect the distillate for later use, decoct the residue with Astragalus, Codonopsis, Rehmannia glutinosa and water for 3 times, 1.5 hours for the first time, 1 hour for the second and third times, and combine the decoctions , filtered, and the filtrate was concentrated to a clear paste with a relative density of 1.08-1.10 (75°C-80°C). After cooling, ethanol was added to make the alcohol content 50-55%. Stir well, cool, stand still, filter, recover ethanol from the filtrate, concentrate to a relative density of 1.08, and set aside; take donkey-hide gelatin and add appropriate amount of water to melt, filter, and combine the filtrate with the above concentrate; make syrup with ...
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