Method for establishing atherosclerosis cell model
A technology of atherosclerosis and cell models, applied in biochemical equipment and methods, organic chemistry, steroids, etc., can solve the problems of time-consuming animal models, unreported atherosclerosis cell models, and cost-consuming problems
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[0043] 1. Chemical synthesis and structural analysis of oxLig-1:
[0044] 1. Synthesis of oxLig-1:
[0045] (1) Create a response:
[0046] 0.500mmol of azelaic acid, 0.1875mmol of DCC and 0.125mmol of catalyst DMAP were dissolved in 15mL of dichloromethane, and 0.125mmol of 7-KC, which was also dissolved in dichloromethane, was added dropwise from a constant pressure funnel, and the molar ratio of each substance was azelaic Acid: DCC: DMAP: 7-KC = 4: 1.5: 1: 1.
[0047]
[0048] The reactant was stirred and reacted at 40° C. for 12 hours, and then refluxed for 12 hours, during which time the reaction was monitored by thin-layer chromatography.
[0049] (2) post-reaction treatment:
[0050] The reaction product was filtered under reduced pressure to remove insoluble urea; extracted 3 times with saturated NaCl, and the organic phase was collected; anhydrous NaCl 2 SO 4 Let dry overnight.
[0051] (3) Sample mixing:
[0052] Weigh the mixed sample silica gel (100-140 m...
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