Short-flow preparation method of micro-sized spherical titanium powder

A technology of spherical titanium powder and short process, which is applied in metal processing equipment, transportation and packaging, etc., to achieve good fluidity, shorten the process flow, and reduce oxidation problems

Active Publication Date: 2010-06-02
江苏金物新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology uses small particles called tetrahedral Titanium Hydride (T1H2) that are used instead of pure metallic magnesium or lithochloride for reducing unwanted reactions such as water loss by reacting them with other chemicals like alcohol or ammonia. These techniques help increase productivity while also minimizing environmental impact on producing materials.

Problems solved by technology

This patented describes methods for producing finely dispersed metallurgically pure tantalum powders that exhibit superior mechanical property compared to existing ones. However, currently available processes require expensive specialty chemicals like ruthenium chloride, making them less efficient when needed over longer periods without losing their quality. Additionally, there exist challenges related to achieving consistently small diameter and highly circular shaped granules while maintaining desired flowability and reducing costs associated with conventional techniques involving ionized vapor deposition.

Method used

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  • Short-flow preparation method of micro-sized spherical titanium powder
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  • Short-flow preparation method of micro-sized spherical titanium powder

Examples

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example 1

[0033] A fine spherical titanium powder with an average particle diameter of 15 μm was prepared.

[0034] Titanium hydride (TiH) with an average particle size of 100 μm 2 ) powder as the raw material, the stable operating radio frequency (RF) plasma power is 50KW, the flow rate of argon working gas is 30 slpm, the flow rate of argon protective gas is 150 slpm, and the system negative pressure is 200 mm Hg. The titanium hydride powder is sent into the high-temperature plasma with the argon gas flow rate of 4 slpm, and the powder delivery rate is 40g / min. After the spheroidization treatment, the fine spherical titanium powder with an average particle size of 15 μm can be obtained by cyclone separation.

example 2

[0036] A fine spherical titanium powder with an average particle diameter of 20 μm was prepared.

[0037] Titanium hydride (TiH) with an average particle size of 150 μm 2 ) powder as the raw material, the stable operating radio frequency (RF) plasma power is 60KW, the flow rate of argon working gas is 40 slpm, the flow rate of argon protective gas is 200 slpm, and the system negative pressure is 230 mm Hg. The titanium hydride powder is sent into the high-temperature plasma with the argon gas with a flow rate of 4.5 slpm, and the powder delivery rate is 50g / min. After the spheroidization treatment, the fine spherical titanium powder with an average particle size of 20 μm can be obtained by cyclone separation.

Embodiment 3

[0039] A fine spherical titanium powder with an average particle diameter of 10 μm was prepared.

[0040] Titanium hydride (TiH) with an average particle size of 50 μm 2) powder as the raw material, the stable operating radio frequency (RF) plasma power is 45KW, the flow rate of argon working gas is 30 slpm, the flow rate of argon protective gas is 200 slpm, and the system negative pressure is 200 mm Hg. The titanium hydride powder is sent into the high-temperature plasma with the argon gas with a flow rate of 4 slpm, and the powder delivery rate is 30g / min. After the spheroidization treatment, the fine spherical titanium powder with an average particle size of 10 μm can be obtained by cyclone separation.

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Abstract

The invention provides a short-flow preparation method of micro-sized spherical titanium powder, which belongs to the technical field of powder preparation. The hydrogenation-dehydrogenation technique and the radio frequency plasma body fusion spheroidization technique are integrated, and the titanium hydride powder is selected as raw material; the titanium hydride powder absorbs heat in the high-temperature plasma and quickly decomposes and dehydrogenates, and the titanium hydride power is cracked and crushed in the process of dehydrogenation to produce the micro-sized titanium powder. By using the method, the processes of the dehydrogenation and the spheroidization of the generated titanium powder are finished in one step directly through the plasma processing, and the short-flow preparation of the micro-sized spherical titanium powder is realized. The invention has the advantages that the hydrogenation-dehydrogenation technique and the radio frequency plasma fusion spheroidization technique are combined, so as to shorten the production flow, enhance the production efficiency and reduce the production cost. Simultaneously, the prepared spherical titanium power has fine and even particles, good liquidity, high sphericity and low oxygen content, thereby the requirements of technical industrial production such as the injection figuration, the gel die casting figuration, and the like are satisfied.

Description

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Claims

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Application Information

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Owner 江苏金物新材料有限公司
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