The application discloses a kind of gel PMMA
slurry, diaphragm
lithium battery and preparation method thereof.Gel PMMA
slurry preparation method includes the following steps: step 1:
methyl methacrylate is added to N-methyl pyrrolidone, and stirred uniformly;Then initiator
azobisisobutyronitrile is added, and stirred min;Subsequently, temperature is raised to 50-70℃, and the heating rate is 3-5℃ / min, keep 30-50min, then continue to heat to 80-90℃, keep 2-4h, and the heating rate is 3-5℃ / min, then cool to
room temperature to obtain PMMA gel;Step 2:
alumina powder is added to N-methyl pyrrolidone, and stirred 30-40min;Then use bar pin type sand mill to sand mill to obtain inorganic
powder solution;Step 3: PMMA gel prepared in step 1 is added to the inorganic
powder solution obtained in step 2, and stirred to mix uniformly;Then
dimethyl carbonate is added, and stirred to obtain gel PMMA
slurry.The prepared gel PMMA coated diaphragm has great adhesion to
pole piece and higher liquid
absorption rate and liquid
retention rate.