Fluidized bed reactor
An ebullating bed reactor and reactor technology, applied in the field of improved three-phase ebullating bed reactor, can solve the problems of high maintenance cost of circulating oil pump, low utilization rate of reactor space, sinking and accumulation of catalyst, etc., and shorten the residence time time, avoid a large amount of carrying out, and prevent the effects of condensation and coking reactions
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Embodiment -1
[0035] According to the structure of the ebullating bed hydrogenation reactor of the present invention, the cold model test of the three-phase separator ebullating bed medium-sized reactor has been carried out. The height of the straight section of the shell = 3000mm, and the effective volume of the shell is 60L. The height of the three-phase separator = 500mm, the diameter of the minimum diameter of the inner cylinder of the separator = 135mm, the diameter of the tapered opening at the lower part of the inner cylinder = 190mm, the height of the lower cone of the inner cylinder = 35mm, the diameter of the smallest diameter of the outer cylinder = 160mm, The opening diameter of the lower section of the outer cylinder = 285mm, the height of the lower section of the outer cylinder = 30mm, the upper opening of the outer cylinder is higher than the upper opening of the inner cylinder, and the bottom position of the lower tapered opening of the outer cylinder is higher than the botto...
Embodiment -2
[0038] On the basis of the cold model test, a hydrodemetallization test of an island atmospheric residue was carried out on a 60L medium-sized unit. Wherein the size of the reactor is the same as in Example 1, and the test conditions and results are shown in Table 2.
Embodiment -3
[0046] The operating conditions are the same as in Example-1. A material distributor is provided in the middle of the straight section of the ebullated bed reactor. The material distributor is a circular secondary distribution plate with a certain opening ratio, and the area of the distribution plate accounts for 0.6% of the cross-sectional area of the reactor. , the opening ratio is 0.5, and the diameter is smaller than the diameter of the reactor, which promotes the distribution of the continuous phase and the dispersed phase, inhibits the formation and coalescence of large bubbles, improves the fluidization quality, and makes the radial velocity distribution of the fluid more uniform. Interference is carried out to improve the mass and heat transfer efficiency and strengthen the process. It can be seen that the mass transfer rate increases when there are internal components, and the fluidization quality is better improved.
[0047] Table 3 Comparison results with and wi...
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