Method for preparing water-retention fertilizer from aquatic plants
A technology for aquatic plants and fertilizers is applied in the field of subsequent utilization and treatment of aquatic plants to achieve the effects of improving soil structure and preventing the degradation of arable land structures.
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example 1
[0029] (1) Raw material selection method:
[0030] Wash and chop the salvaged water hyacinth, dry, crush, and sieve, and select 20-40 mesh hay powder for later use;
[0031] (2) Chemical modification method of aquatic plants (preparation of carboxyl fiber of aquatic plants):
[0032] Add 4g of water hyacinth powder and 80mL of 95% industrial ethanol mixed solution containing 3g of urea and 3gKOH into a 250mL three-neck flask, stir well, and place in a refrigerator at 2°C for 15h; take it out and place it in a heating mantle, and add 4g of Chloroacetic acid, when the temperature rises to 70°C, stir at constant temperature for 1.5h; at 70°C, continue the reaction, start to cool down after 1h, suction filter after the temperature drops to 30°C, and wash the filter cake 3 times with 85% ethanol aqueous solution. Dry at 60°C for 4h, grind the solid finely and set aside.
[0033] (3) Preparation method of water-retaining fertilizer:
[0034] Measure 100mL of distilled water into ...
example 2
[0036] The difference between this example and Example 1 is that the amount of chloroacetic acid is 2.0 g, the reaction temperature is 60° C., and the reaction time is 3 hours. Other preparation steps are the same as Example 1. Relative to the water hyacinth matrix, the potassium content was 11.3%, and the nitrogen content was 10.2%. The water absorption factor of this example is 20.
example 3
[0038] The difference between this example and Example 1 is that the amount of chloroacetic acid is 6.0 g, the reaction temperature is 50° C., and the reaction time is 8 hours. Other preparation steps are the same as Example 1. Relative to the water hyacinth matrix, the potassium content is 13.5% and the nitrogen content is 9.5%. The water absorption ratio of this example is 62.
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