Germanium viscose fiber and preparation method thereof
A viscose fiber and viscose technology, which is applied in fiber treatment, spinning solution preparation, and artificial filaments made of viscose, can solve the problems of insufficient moisture absorption and ventilation, and can not be naturally degraded, so as to reduce functionality and Effect of appearance, good textile processing performance, cost reduction effect
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Embodiment 1
[0032] Embodiment 1, the preparation method of germanium viscose fiber, comprises the following steps:
[0033] a, the preparation of germanium ore slurry: take the germanium ore whose particle diameter is 125nm, add in germanium ore relative to the surfactant dialkyl dimethyl ammonium chloride of 0.3% by weight of germanium ore and relative to the weight of germanium ore 0.3% dispersant polysiloxane quaternary ammonium salt, and then add deionized water to configure germanium ore slurry with a concentration of 25%;
[0034] b. Preparation of dissolving viscose: using hemp pulp as raw material, through dipping, pressing, pulverizing, aging, yellowing and dissolving processes, adding denaturant alkyl polyamine in the dissolving process to obtain dissolving viscose, alkyl polyamine The addition of amine is 2% of the alpha cellulose weight in the viscose;
[0035] c, the preparation of germanium slurry: add dissolving viscose in the germanium ore slurry, obtain mixture, the weig...
Embodiment 2
[0043] Embodiment 2, germanium viscose fiber and preparation method thereof, comprises the following steps:
[0044] a, the preparation of germanium ore slurry: take the germanium ore that particle size is 95nm, add in germanium ore relative to the surfactant dialkyl dimethyl ammonium chloride of 0.2% by weight of germanium ore and relative to the weight of germanium ore 1.2% sodium tripolyphosphate, then add deionized water to configure germanium ore slurry with a concentration of 20%;
[0045] b. Preparation of dissolving viscose: using hemp pulp as raw material, through dipping, squeezing, pulverizing, aging, yellowing and dissolving processes, adding denaturant alkylpolyamine in the dissolving process to obtain dissolving viscose, alkyl The addition of polyamine is 1.8% of the alpha cellulose weight in the viscose;
[0046] c, preparation of germanium slurry: adding dissolving viscose in the germanium ore slurry to obtain a mixture, the weight ratio of the germanium ore s...
Embodiment 3
[0054] Embodiment 3, germanium viscose fiber and preparation method thereof, comprises the following steps:
[0055] a, the preparation of germanium ore slurry: take the germanium ore that particle size is 85nm, in germanium ore, add the surfactant polyalkyl trimethylammonium chloride relative to germanium ore weight 0.6% and relative to germanium ore weight 0.8% sodium tripolyphosphate, then add deionized water to configure germanium ore slurry with a concentration of 30%;
[0056] b. Preparation of dissolving viscose: using hemp pulp as raw material, through dipping, squeezing, pulverizing, aging, yellowing and dissolving processes, adding denaturant alkylpolyamine in the dissolving process to obtain dissolving viscose, alkyl The addition of polyamine is 2.2% of the alpha cellulose weight in the viscose;
[0057] c, the preparation of germanium slurry: add dissolving viscose in the germanium ore slurry, obtain mixture, the weight ratio of germanium ore slurry and dissolving...
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