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Water-soluble OP wax emulsion and preparation method thereof

A wax emulsion and water-soluble technology, applied in the field of water-soluble OP wax emulsion and its preparation, can solve the problems of residual influence, high wax cost, restricting development, etc., and achieve the effects of low cost, good rheology and good coverage.

Active Publication Date: 2013-03-20
哈尔滨绿科科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Before the present invention, our company and the society all produced and applied conventional wax emulsions on the market, but due to the use of a single surfactant or cationic surfactant as an emulsifier, the stability of the finished product was relatively poor, and the amount of emulsifier used Failure to find a reasonable ratio leads to excessive residues that affect the environment and cannot meet the requirements of smoking materials, and other problems such as high wax costs also restrict the healthy development of the industry

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] The raw material composition of present embodiment:

[0024] OP wax, milky white sliced ​​solid, 24.5 parts,

[0025] Fatty alcohol polyoxyethylene ether, colorless or yellow transparent oil, 9 parts,

[0026] Fatty alcohol polyoxyethylene ether phosphate, colorless or yellow transparent oil, 1.5 parts,

[0027] Deionized water, colorless transparent liquid, 65 parts,

[0028] Wherein, the HLB value of the OP wax is 11, the molecular weight is 260-350, and the density is 0.9-0.95g / cm 3 The fatty alcohol polyoxyethylene ether is a nonionic surfactant with an HLB value of 14; the fatty alcohol polyoxyethylene ether phosphate salt is a kind of anionic surfactant HLB value of sodium salt or potassium salt 3.5.

[0029] The OP wax is a synthetic wax, and the emulsifier is a composite emulsifier prepared from fatty alcohol polyoxyethylene ether and fatty alcohol polyoxyethylene ether phosphate in a ratio of 6.

[0030] The preparation method of this embodiment is:

[00...

Embodiment 2

[0035] The raw material composition of present embodiment:

[0036] OP wax, milky white sliced ​​solid, 26.5 parts,

[0037] Fatty alcohol polyoxyethylene ether, colorless or yellow transparent oil, 3 parts,

[0038] Fatty alcohol polyoxyethylene ether phosphate, colorless or yellow transparent oil, 0.5 parts,

[0039] Deionized water, colorless transparent liquid, 70 parts,

[0040] Wherein, the HLB value of the OP wax is 11, the molecular weight is 260-350, and the density is 0.9-0.95g / cm 3 The fatty alcohol polyoxyethylene ether is a nonionic surfactant with an HLB value of 14; the fatty alcohol polyoxyethylene ether phosphate salt is a kind of anionic surfactant HLB value of sodium salt or potassium salt 3.5.

[0041] The OP wax is a synthetic wax, and the emulsifier is a composite emulsifier prepared from fatty alcohol polyoxyethylene ether and fatty alcohol polyoxyethylene ether phosphate in a ratio of 6.

[0042] The preparation method of this embodiment is:

[00...

Embodiment 3

[0047] The raw material composition of present embodiment:

[0048] OP wax, milky white sliced ​​solid, 28 parts,

[0049] Fatty alcohol polyoxyethylene ether, colorless or yellow transparent oil, 6 parts,

[0050] Fatty alcohol polyoxyethylene ether phosphate, colorless or yellow transparent oil, 1 part,

[0051] Deionized water, colorless transparent liquid, 65 parts,

[0052] Wherein, the HLB value of the OP wax is 11, the molecular weight is 260-350, and the density is 0.9-0.95g / cm 3The fatty alcohol polyoxyethylene ether is a nonionic surfactant with an HLB value of 14; the fatty alcohol polyoxyethylene ether phosphate salt is a kind of anionic surfactant HLB value of sodium salt or potassium salt 3.5.

[0053] The OP wax is a synthetic wax, and the emulsifier is a composite emulsifier prepared from fatty alcohol polyoxyethylene ether and fatty alcohol polyoxyethylene ether phosphate in a ratio of 6.

[0054] The preparation method of this embodiment is:

[0055] (1...

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Abstract

The invention relates to a water-soluble OP wax emulsion and a preparation method thereof, belonging to the technical field of novel wax emulsion materials. The OP wax emulsion is prepared from the following components in parts by weight: 19.5-32 parts of OP wax, 2.54-9.25 parts of fatty alcohol-polyoxyethylene ether, 0.45-1.58 parts of fatty alcohol-polyoxyethylene ether phosphate and 65-70 parts of deionized water which are added and stirred uniformly in sequence in a reaction kettle for heating and melting with an agent-in-oil method. The OP wax emulsion prepared with the method provided by the invention has the advantages of high stability reaching 98-100 percent, favorable dispersibility and rheological behaviour, no layering after diluted by water of any proportion, small average particle diameter less than 0.4mum, no holes on the surface, no sediments at the bottom, favorable uniformity and coverage after film formation, recombination with water solutions or emulsion fluid of other substances, safety, high efficiency, economy, convenience, lower cost and favorable popularization and application value on the market.

Description

technical field [0001] The invention relates to a wax emulsion and a preparation method thereof, in particular to an emulsifier using OP wax, nonionic surfactant fatty alcohol polyoxyethylene ether and anionic surfactant fatty alcohol polyoxyethylene ether phosphate The produced water-soluble OP wax emulsion and its preparation method. Background technique [0002] There is a big gap between the development and application of emulsified paraffin in my country and foreign countries. The departments that can use emulsifying wax almost all use unreasonable substitutes, and the potential market capacity of emulsifying wax in my country is huge, so this invention is of great significance. [0003] Because emulsified wax does not need to be melted by heating or dissolved by solvent, it has uniform film formation and good coverage, and is easy to be used in combination with aqueous solutions or emulsions of other substances. It has the advantages of safety, high efficiency, econom...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L91/06C08J3/05
Inventor 张立伟张伟赵国宝于洋王乃军王长胜李玉良李洪刚刘志刚
Owner 哈尔滨绿科科技有限公司
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