Preparation method of microporous membrane with hydrophilicity and hydrophobicity
A microporous membrane and hydrophobic technology, applied in the field of preparation of microporous membranes, can solve the problems of easy change of stretched network pores, affecting filtration accuracy, and high technical difficulty, achieving stable and uniform shape of membrane pores, improving filtration efficiency, The effect of high filtration efficiency
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Embodiment 1
[0020] A method for preparing a microporous membrane having both hydrophilicity and hydrophobicity, comprising the following steps:
[0021] (1) Put dimethylformamide in a jar, add 100g of polyethersulfone, add 80g of polyethylene glycol 400 as an additive, and 13g of glycerin, configure it to be fully dissolved, then airtightly stand for defoaming to obtain Casting solution;
[0022] (2) Control the temperature in the steam zone at 60°C and the relative humidity at 100%;
[0023] (3) Dip-coat the casting solution onto a polyester non-woven fabric with a thickness of 40 μm, and use a scraper to control the coating thickness to 200 μm. After evaporating for 5 minutes, measure the first bubble point pressure with a thickness of 25 μm using absolute ethanol as a medium The PTFE micro-membrane pores of 0.10MPA are compounded on one side on the polyester non-woven fabric soaked in the casting liquid. After being flattened by the device, they enter the steam area to form a film. Af...
Embodiment 2
[0025] A method for preparing a microporous membrane having both hydrophilicity and hydrophobicity, comprising the following steps:
[0026] (1) Preparation of casting solution for microporous membrane of hydrophilic support layer: first, dissolve sulfonated polyether sulfone in dimethylformamide solvent, and add polyvinyl acid as an additive to form a three-component membrane material / solvent / additive Element film making liquid, airtight defoaming, obtain coating liquid, the concentration of membrane material in this coating liquid is 5wt%, the concentration of additive is 2wt%;
[0027] (2) Phase conversion and composite film formation: Install polyester non-woven fabric on continuous film casting equipment, put the casting film solution into the material tank, use a scraper to dip the casting film solution evenly on the polyester non-woven fabric, After evaporating the solvent in the casting solution, compound a polytetrafluoroethylene microporous membrane on one side of th...
Embodiment 3
[0029] A method for preparing a microporous membrane having both hydrophilicity and hydrophobicity, comprising the following steps:
[0030] (1) Preparation of the casting solution for the microporous membrane of the hydrophilic support layer: firstly, nylon 6 is dissolved in formic acid solvent, and the additive calcium chloride is added to form a ternary membrane-making solution of membrane material / solvent / additive. Bubble, obtain coating solution, the concentration of membrane material in this coating solution is 18wt%, and the concentration of additive is 3wt%;
[0031] (2) Phase conversion and composite film formation: Install polyester non-woven fabric on continuous film casting equipment, put the casting film solution into the material tank, use a scraper to dip the casting film solution evenly on the polyester non-woven fabric, After evaporating the solvent in the casting solution, compound a polytetrafluoroethylene microporous membrane on one side of the polyester no...
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