Process for extracting fluoride-free shrimp oil from dried antarctic krill
An Antarctic krill and shrimp oil technology, applied in the production of fat oil/fat and fat production, can solve the problems of large waste of resources, low protein yield, high fluorine content harmful to human health, etc., to achieve high yield and improve quality Effect
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Embodiment 1
[0023] Example 1 Extracting fluorine-free shrimp oil from Antarctic krill
[0024] The steps are:
[0025] (1) Dried Antarctic krill 100g, add acetone 550ml, extract 3 times at 25°C, extract 1h each time, filter out the dried Antarctic krill; combine the three extracts (1400ml), at 45°C , Acetone was removed by rotary evaporation at -0.09Mpa to obtain 6.20g of shrimp oil, the fluorine content of which was 114.332ug according to the national standard GB / T5009.18-2003.
[0026] (2) Shrimp dregs (85g) were obtained by filtration after the last extraction above, and 550ml of 95% ethanol was added to the shrimp dregs, extracted three times at 25°C, each time for 1 hour, and filtered to filter out the dried Antarctic krill; The three extracts (1400ml) were combined, and the ethanol was removed by rotary evaporation at 55°C and -0.09Mpa to obtain 43.75g of concentrate, the fluorine content of which was 658.45ug.
[0027] (3) Add 220ml of acetone to the concentrate obtained in step (2...
Embodiment 2
[0029] Example 2 Extracting fluorine-free shrimp oil from Antarctic krill
[0030] The steps are:
[0031] (1) Dry Antarctic krill 100g, add acetone 600ml, extract 3 times at 35°C, extract 1h each time, filter the dried Antarctic krill; combine the three extracts (1500ml), at 50°C , Acetone was removed by rotary evaporation at -0.08Mpa, and 6.41g of shrimp oil was obtained. According to the national standard GB / T5009.18-2003, the fluorine content was 118.110ug.
[0032] (2) Shrimp dregs (85g) were obtained by filtration after the last extraction above, and 600ml of 95% ethanol was added to the shrimp dregs, and extracted at 35°C for 3 times, 1 hour each time, and the dried Antarctic krill was filtered out after each extraction; The three extracts (1500ml) were combined, and the ethanol was removed by rotary evaporation at 60°C and -0.08Mpa to obtain 45.10g of concentrate, the fluorine content of which was 662.333ug.
[0033] (3) Add 225ml of acetone to the concentrate obtain...
Embodiment 3
[0035] Example 3 Extracting fluorine-free shrimp oil from Antarctic krill
[0036] The steps are:
[0037] (1) Add 100g of dried Antarctic krill, add 650ml of acetone, extract 3 times at 20°C, extract for 1 hour each time, and filter out the dried Antarctic krill after each extraction; combine the three extracts (1750ml) at 55°C, Acetone was removed by rotary evaporation at -0.07Mpa to obtain 6.57g of shrimp oil, the fluorine content of which was 119.452ug.
[0038] (2) Shrimp dregs (83g) were obtained by filtering after the last extraction above. Add 650ml of absolute ethanol to the shrimp dregs and extract 3 times at 20°C for 1 hour each time. After each extraction, filter out the dried Antarctic krill The three extracts (1750ml) were combined, and the ethanol was removed by rotary evaporation at 65°C and -0.07Mpa to obtain 39.5g of concentrate, the fluorine content of which was 644.278ug.
[0039] (3) Add 200ml of acetone to the concentrate obtained in step (2), stir and ...
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