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Automatic glaze spraying technology for electronic vacuum metallized ceramic surface

A technology of metallized ceramics and vacuum electronics, which is applied in the field of automatic glaze spraying process on the surface of vacuum electronic metallized ceramics, can solve the problems of flow glaze and uneven thickness of glaze layer, difficult control of production operation, uneven thickness of glaze layer, etc. Achieve the effect of good air tightness, easy operation and reliable quality

Active Publication Date: 2013-10-23
湖南湘瓷科艺有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Thermal spraying is to spray the glaze on the heated porcelain parts. The heat of the porcelain body volatilizes the water in the glaze sprayed on the porcelain body so that the glaze powder can adhere to the porcelain body. The difference in height causes defects such as orange peel, flow glaze, wrinkling and uneven thickness of the glaze layer. Not only is it difficult to control in the production operation, but also consumes a lot of heat energy. 0.8~1.6μm), the water absorption rate is less than 0.3%, the water volatilization of the glaze is very slow at room temperature, and it is not easy to adhere to the glaze slurry, causing defects such as flow glaze and uneven thickness of the glaze layer

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A. Preparation of glaze slurry spraying agent

[0026] 1) Glaze slurry iron removal

[0027] For the selected glaze slurry, remove the iron in the glaze slurry by filtering with a 200 mesh sieve;

[0028] 2) Prepare the suspending agent

[0029] 70% bentonite and 30% quartz are evenly mixed, calcined at 1200°C, processed into a slurry, and filtered with a 200-mesh sieve to prepare a suspension with a water content of 60%;

[0030] 3) Preparation of glaze slurry spraying agent

[0031] 8% of suspending agent, 0.1% of water glass and 0.2% of sodium polyacrylate were stirred evenly to prepare a glaze slurry additive, which was added to 91.7% of the glaze slurry after iron removal, and stirred to a concentration of 55 o Bé, the glaze slurry spraying agent that moisture content is 38%, above all is weight ratio;

[0032] B. Install the mold on the machine

[0033] Install the sintered qualified ceramic workpiece on the corresponding mold and fix it on the rotating shaf...

Embodiment 2

[0044] A. Preparation of glaze slurry spraying agent

[0045] 1) Glaze slurry iron removal

[0046] For the selected glaze slurry, use a 200-mesh sieve to remove iron in the glaze slurry.

[0047] 2) Prepare the suspending agent

[0048] 70% bentonite and 30% quartz are uniformly mixed, calcined at 1200°C, processed into a slurry and filtered with a 200-mesh sieve to prepare a suspension with a water content of 60%.

[0049] 3) Preparation of glaze slurry spraying agent

[0050] 8% of suspending agent, 0.15% of water glass and 0.25% of sodium polyacrylate were stirred and mixed evenly to make a glaze slurry additive, added to 91.6% of the glaze slurry after iron removal, and stirred to make a concentration of 60 o Bé, a glaze spraying agent with a moisture content of 32%.

[0051] B. Install the mold on the machine

[0052] Install the sintered qualified ceramic workpiece on the corresponding mold and fix it on the rotating shaft of the automatic glaze spraying machine. ...

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Abstract

The invention relates to an automatic glaze spraying technology for an electronic vacuum metallized ceramic surface, which has the key points of filtering raw glaze slip by a 200-mesh screen to remove iron; stirring and mixing 2-20% of suspending agent, 0-0.3% of water glass and 0-0.4% of sodium polyacrylate to form glaze slip additive; adding the glaze slip additive into 79.3-98% of glaze slip which is treated by deironing, and stirring to prepare glaze slip spraying agent with 50-70 o Be and the moisture content of 30-45%; setting the operating parameters of a glaze spraying machine, and spraying glaze for 4-10 times; and naturally drying for 1-2h at the room temperature. The automatic glaze spraying technology is simple in glaze spraying technology, and the prepared glaze slip spraying agent is proper in fluidity on the surface of a workpiece; the technology is convenient to operate and control; the glaze slip sprayed on the surface of the workpiece is good in compactness and smoothness; a glaze layer stuck on the surface of the workpiece is even in thickness; the produced metallized ceramic can be welded with metal, so that a composite ceramic part with firm connection, good air tightness, reliable quality and stable performances can be formed; and product quality and production efficiency are improved, and the production cost and energy consumption are reduced.

Description

technical field [0001] The invention relates to a glaze spraying process, in particular to an automatic glaze spraying process for vacuum electronic metallized ceramic surfaces. Background technique [0002] General ceramics: The entire porcelain body needs to be glazed, and the glaze is applied on the green body with high water absorption rate before the porcelain is fired, and the vacuum electronic metallized ceramics is a key structural component of the vacuum interrupter, and the sintering temperature is high. The dimensional tolerance is required to be small, and the sintered ceramics need to be machined according to the drawings in the follow-up. Glazing can only be applied after the semi-finished ceramics have been processed to pass the dimensions and cleaned. And it is required to have glaze in a certain area of ​​the outer surface of the product, and the outer surface is within a certain distance from both ends (generally about 2mm) and the inner wall is not allowed...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B41/86
Inventor 陈金华杨润华李微冯波
Owner 湖南湘瓷科艺有限公司
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