Unlock instant, AI-driven research and patent intelligence for your innovation.

A powdery composition containing sodium ethoxylated alkyl sulfate and its preparation method

A technology of sodium ethoxylated alkyl sulfate and composition, which is applied in the field of powdery compositions containing sodium ethoxylated alkyl sulfate, and can solve the problems of reduced production efficiency, difficulty in applying powder, large material loss and the like , to achieve mild washing effect, prevent mutual adhesion, and good hard water resistance.

Active Publication Date: 2015-09-09
ZANYU TECH GRP CO LTD +1
View PDF5 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1. The product form of ethoxylated alkyl sodium sulfate is relatively special. When the concentration is 70%, it is a flowing gel paste; when the concentration is less than 28%, it is a transparent liquid; It is a gel paste that is difficult to flow, so it is difficult to apply in powder; and sodium ethoxylated alkyl sulfate has sticky characteristics, even if it is produced by agglomeration molding process, the dosage will be limited (generally not more than 2 %);
[0004] 2. Sodium ethoxylated alkyl sulfate is easy to decompose at high temperature, and the main washing powder drying process currently used is high-tower spraying (produced by high-temperature hot air at 250-350 ° C), which cannot be used for ethoxylation Drying and powdering of sodium alkyl sulfate
[0005] Chinese patent CN101942082B discloses a preparation method of powdery AES or AES mixture, which proposes: AES (ethoxylated alkyl sodium sulfate) or AES mixture is dehydrated and dried (water content is less than 5%), and then frozen to produce powder; the weak point of this preparation method is:
[0006] 1. It needs to use special drying and freezing equipment for production, which consumes a lot of energy;
[0007] 2. During the production process, AES will adhere to the inner wall of the drying and freezing equipment and decompose within a period of time, resulting in large material loss;
[0008] 3. It is necessary to regularly clean the drying and freezing equipment to remove the AES adhered to the inner wall of the equipment, which not only reduces the production efficiency, but also produces a large amount of washing wastewater and pollutes the environment

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A powdery composition containing sodium ethoxylated alkyl sulfate, comprising: 420 kg of sodium ethoxylated alkyl sulfate, 100 kg of anhydrous sodium sulfate, and 480 kg of 4A zeolite;

[0029] The molecular formula of the ethoxylated sodium alkyl sulfate is R(CH 2 CH 2 O)nOSO 3 Na, wherein R is an alkyl carbon chain with 12-14 carbon atoms, and n is 1.

[0030] The preparation method of above-mentioned powdery composition containing sodium ethoxylate alkyl sulfate, comprises the following steps:

[0031] Step 1: Stir and mix the ethoxylated alkyl sodium sulfate and anhydrous sodium sulfate evenly, then age for 1.5 hours; the temperature is 10-15°C;

[0032] The second step, add the coating agent and stir to mix evenly;

[0033] In the third step, the finished product is obtained after being sieved through a 40-mesh sieve after pulverization; the content of sodium ethoxylated alkyl sulfate in the finished product is 29.4%.

Embodiment 2

[0035] A powdery composition containing sodium ethoxylated alkyl sulfate, comprising: 430 kg of sodium ethoxylated alkyl sulfate, 300 kg of anhydrous sodium carbonate, and 270 kg of bentonite;

[0036] The molecular formula of the ethoxylated sodium alkyl sulfate is R(CH 2 CH 2 O)nOSO 3 Na, wherein R is an alkyl carbon chain with 16-18 carbon atoms, and n is 2.

[0037] The preparation method of above-mentioned powdery composition containing sodium ethoxylate alkyl sulfate, comprises the following steps:

[0038] The first step is to mix the ethoxylated alkyl sodium sulfate and anhydrous sodium carbonate evenly and then age for 0.5h; the temperature is 0-5°C;

[0039] The second step, add bentonite and stir to mix evenly;

[0040] In the third step, the finished product is obtained after being pulverized and sieved through a 30-mesh sieve; the content of sodium ethoxylated alkyl sulfate in the finished product is 30.1%.

Embodiment 3

[0042] A powdery composition containing sodium ethoxylated alkyl sulfate, comprising the following components: 400 kg of sodium ethoxylated alkyl sulfate, 100 kg each of anhydrous sodium carbonate and anhydrous sodium sulfate, and 400 kg of diatomaceous earth;

[0043] The molecular formula of the ethoxylated sodium alkyl sulfate is R(CH 2 CH 2 O)nOSO 3 Na, wherein R is an alkyl carbon chain with 22 carbon atoms, and n is 1.

[0044] The preparation method of above-mentioned powdery composition containing sodium ethoxylate alkyl sulfate, comprises the following steps:

[0045] Step 1: Stir and mix ethoxylated alkyl sodium sulfate, anhydrous sodium carbonate and anhydrous sodium sulfate evenly, then age for 1 hour at a temperature of 25-30°C;

[0046] The second step, add diatomaceous earth and stir to mix evenly;

[0047] In the third step, the finished product is obtained after being pulverized and sieved through a 40-mesh sieve, and the content of sodium ethoxylated alky...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a powdery composition containing ethoxylated sodium alkyl sulfate, and a preparation method of the composition. The invention aims at providing the composition which needs to contain the ethoxylated sodium alkyl sulfate, has the characteristics of good mobility and difficulty in adhesion, and can be directly used for a washing powder distribution technique. The method provided by the invention has the characteristics of simple technique, energy saving and environmental friendliness, and high production efficiency. According to the technical scheme, the composition containing the powdery ethoxylated sodium alkyl sulfate comprises the following components in percentage by weight: 20-45% of ethoxylated sodium alkyl sulfate, 10-30% of water-absorbing auxiliaries, and 20-50% of wrapping agent. The preparation method for the powdery composition containing ethoxylated sodium alkyl sulfate comprises the following steps: I. evenly mixing the ethoxylated sodium alkyl sulfate and the water-absorbing auxiliaries, and aging for 0.5-2 hours; II. adding the wrapping agent and evenly mixing; and III. crushing and then screening through a sieve with 10-50 meshes.

Description

technical field [0001] The invention relates to a powdery composition containing sodium ethoxylated alkyl sulfate and a preparation method thereof. Background technique [0002] Sodium ethoxylated alkyl sulfate is an anionic surfactant based on natural oil. It has excellent decontamination, emulsification, foaming and anti-hard water properties. It is widely used in shampoos, body washes, dishwashing detergents and other liquids. in washing products. However, sodium alkylbenzene sulfonate is usually used as a surfactant in washing powder at present (sodium ethoxylated alkyl sulfate is rarely used), and the reasons are: [0003] 1. The product form of ethoxylated alkyl sodium sulfate is relatively special. When the concentration is 70%, it is a flowing gel paste; when the concentration is less than 28%, it is a transparent liquid; It is a gel paste that is difficult to flow, so it is difficult to apply in powder; and sodium ethoxylated alkyl sulfate has sticky characteristi...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C11D1/16C11D3/60C11D3/10C11D3/08C11D3/04
Inventor 夏雄燕雷小英方灵丹华文高黄亚茹方银军
Owner ZANYU TECH GRP CO LTD