Measurement method for substance variable temperature magnetic susceptibility and measurement device thereof
A measurement method and technology of magnetic susceptibility, which is applied in the field of measurement method and device for measuring material magnetic susceptibility, and can solve problems such as limitations and large errors
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Embodiment 1
[0055] In this example, see figure 1 The material magnetic susceptibility measuring device is composed of an electronic balance 1 with a hook, a balance support 2, a sample tube 4, a magnetic field generator and a magnetic susceptibility analysis system 14, the balance support supports the electronic balance 1, and the sample tube 4 is capable of loading the tested sample 5 has a bottomed container, the sample tube 4 is suspended on the hook of the electronic balance 1, the sample tube 4 is arranged in the magnetic field environment formed by the magnetic field generator, the weighing data signal output terminal of the electronic balance 1 and the magnetic susceptibility analysis system 14 The input end is connected, and the magnetic susceptibility information of the sample to be tested is processed and output by the magnetic susceptibility analysis system 14, and the sample tube 4 is suspended in the inner cavity of the heating furnace formed by a vertically arranged cylindric...
Embodiment 2
[0060] It is basically the same as the aforementioned first embodiment, and the special features are:
[0061] In this embodiment, a pure titanium sample is used as the tested sample 5, and the magnetic field generator adopts a superconducting coil for excitation, and by adjusting the shape and configuration of the superconducting coil, a magnetic field with a magnetic field gradient product stable region is generated, so that the magnetic field in the magnetic field gradient The magnetic force suffered by the matter in the product constant area is a constant value. Using a superconducting coil to excite the magnet, a similar magnetic field can be constructed by adjusting the shape and structure of the superconducting coil, without using the auxiliary wedge-shaped magnetic conducting pole head 13 in the first embodiment. When using the material magnetic susceptibility measuring device of this embodiment to measure the variable temperature magnetic susceptibility of pure titani...
Embodiment 3
[0064] It is basically the same as the aforementioned first embodiment, and the special features are:
[0065] In this embodiment, a single crystal aluminum sample is used as the test sample 5, and the magnetic susceptibility of the (100) crystal plane is measured, wherein the gradient magnetic field is generated by a superconducting coil. When measuring the variable temperature magnetic susceptibility of a single crystal aluminum sample, first adjust the input current in the superconducting coil, and adjust the magnetic field gradient product to 400T 2 / m. Then put a single crystal aluminum sample with a known mass m=1.0000g into the sample tube 4, hang it in the uniform area of the magnetic field gradient product, and make the measured crystal plane (100) perpendicular to the direction of the magnetic field, and place the whole device in a vacuum In the sealing device 6, vacuumize to 10 -3 Pa, exclude air interference. Then adjust the heating current of the temperature c...
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