Preparation method of fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract
A fruit and vegetable cleaning agent, the technology of Schisandra chinensis, which is applied in the directions of chemical instruments and methods, surface active non-soap compounds and washing compositions, detergent compositions, etc. The bacteriostatic effect is not as good as the bacteriostatic effect, and the final product contains many impurities, etc., to achieve the effect of sterilization and broad antibacterial spectrum, good bactericidal effect, and prolonging storage and preservation time and shelf life.
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[0031] A preparation method of a fruit and vegetable cleaning agent compounded by Schisandra chinensis extract and Camellia oleifera cake extract, comprising the following steps:
[0032] 1) Extraction: Extract the southern Schisandra powder with a mixture of ethanol and acetone with a volume ratio of (50~55): 100 as the extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain the flavonoid concentration 0.8~1.0mg / mL crude extract solution of Schisandra chinensis;
[0033] Extract the camellia oleifera cake powder with an ethanol solution with a volume concentration of 60-65% as an extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain a crude oil-tea oleifera cake with a saponin concentration of 1.6-2.1 mg / mL. extract solution;
[0034] 2) Purification: firstly pretreat the resin, put the resin into a column, and adjust the pH value of the crude extract solution of Schisandra chinensis and the crud...
Embodiment 1
[0046] Example 1 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract
[0047] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 60-70°C until the water content is below 8%, pulverize, and pass through a 20-mesh sieve to obtain Schisandra chinensis powder, which is sealed and stored for later use;
[0048] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;
[0049] 2) Extraction: Place the Schisandra chinensis powder obtained in the previous step in a condensation reflux device (this device is convenient for the recovery of the extractant in the subsequent vacuum distillation process), and add ethanol and acetone with a volume ratio of (50~55):100 The mixed solution is used as the extractant, the ratio of solid to liquid is 1g: (40~50) mL, after leachin...
Embodiment 2
[0054] Example 2 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract
[0055] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 65°C until the water content is below 8%, pulverize, pass through a 20-mesh sieve to obtain Schisandra chinensis powder, seal and store for later use;
[0056] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;
[0057] 2) Extraction: Put the southern Schisandra powder obtained in the previous step in a condensation reflux device (this device facilitates the recovery of the extractant in the subsequent vacuum distillation process), and add a mixture of ethanol and acetone with a volume ratio of 50:100 as Extractant, the ratio of solid to liquid is 1g: 50mL, after leaching at 75°C for 3.0h, cooling, filtering to take the filtra...
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