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Preparation method of fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract

A fruit and vegetable cleaning agent, the technology of Schisandra chinensis, which is applied in the directions of chemical instruments and methods, surface active non-soap compounds and washing compositions, detergent compositions, etc. The bacteriostatic effect is not as good as the bacteriostatic effect, and the final product contains many impurities, etc., to achieve the effect of sterilization and broad antibacterial spectrum, good bactericidal effect, and prolonging storage and preservation time and shelf life.

Inactive Publication Date: 2017-11-21
ZHONGKAI UNIV OF AGRI & ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still many problems in the industrial application of its antibacterial active ingredients
For example: the antibacterial effect of the antibacterial active ingredients is affected by the pH value of the solvent; the ordinary extraction process will cause a large loss of antibacterial active ingredients in Schisandra chinensis and camellia oleifera cake, the antibacterial effect is not ideal, and the end product contains more impurities, etc. Difficult problem; with the same dosage, the antibacterial effect of the antibacterial agent extracted from Schisandra chinensis and Camellia oleifera cake is not as good as that of chemically synthesized antibacterial agent
For the antibacterial active ingredients of Schisandra chinensis, the optimization of extraction process, the separation of effective antibacterial ingredients, the antibacterial properties, and the application of antibacterial active ingredients in fruit and vegetable food cleaning agents are not sufficient.
Therefore, the development and use of Schisandra chinensis extract and Camellia oleifera cake extract as natural fruit and vegetable food cleaning agents still need to solve the problems of poor stability after long-term storage, reduced antibacterial activity, and insufficient application research.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0031] A preparation method of a fruit and vegetable cleaning agent compounded by Schisandra chinensis extract and Camellia oleifera cake extract, comprising the following steps:

[0032] 1) Extraction: Extract the southern Schisandra powder with a mixture of ethanol and acetone with a volume ratio of (50~55): 100 as the extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain the flavonoid concentration 0.8~1.0mg / mL crude extract solution of Schisandra chinensis;

[0033] Extract the camellia oleifera cake powder with an ethanol solution with a volume concentration of 60-65% as an extractant, filter the extract, take the filtrate, and then concentrate the filtrate to obtain a crude oil-tea oleifera cake with a saponin concentration of 1.6-2.1 mg / mL. extract solution;

[0034] 2) Purification: firstly pretreat the resin, put the resin into a column, and adjust the pH value of the crude extract solution of Schisandra chinensis and the crud...

Embodiment 1

[0046] Example 1 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract

[0047] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 60-70°C until the water content is below 8%, pulverize, and pass through a 20-mesh sieve to obtain Schisandra chinensis powder, which is sealed and stored for later use;

[0048] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;

[0049] 2) Extraction: Place the Schisandra chinensis powder obtained in the previous step in a condensation reflux device (this device is convenient for the recovery of the extractant in the subsequent vacuum distillation process), and add ethanol and acetone with a volume ratio of (50~55):100 The mixed solution is used as the extractant, the ratio of solid to liquid is 1g: (40~50) mL, after leachin...

Embodiment 2

[0054] Example 2 A preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract

[0055] 1) Pretreatment: Wash and drain the fresh fruit of Schisandra chinensis, air-dry at 65°C until the water content is below 8%, pulverize, pass through a 20-mesh sieve to obtain Schisandra chinensis powder, seal and store for later use;

[0056] Pulverize the camellia oleifera cake and pass through a 20-mesh sieve to obtain the camellia oleifera cake powder, which is sealed and stored for later use;

[0057] 2) Extraction: Put the southern Schisandra powder obtained in the previous step in a condensation reflux device (this device facilitates the recovery of the extractant in the subsequent vacuum distillation process), and add a mixture of ethanol and acetone with a volume ratio of 50:100 as Extractant, the ratio of solid to liquid is 1g: 50mL, after leaching at 75°C for 3.0h, cooling, filtering to take the filtra...

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Abstract

The invention discloses a preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract. The invention adopts the ethanol / acetone method extract of schisandra chinensis and the ethanol method extract of camellia oleifera cake, combined with resin separation technology , respectively purify the extract of Schisandra chinensis and the extract of camellia oleifera, after purifying the above extracts, freeze-dry to obtain extract powder, and mix the extract powder of schisandra chinensis and camellia oleifera cake to obtain a compound fruit and vegetable cleaning agent. The compound fruit and vegetable cleaning agent of the present invention can ensure that unhygienic things such as soil, dirt, pesticides, germs, insect eggs, etc. on the surface of fruits and vegetables are cleaned, and does not affect the freshness of fruits and vegetables during the shelf life, and has biological High safety, low toxicity, high efficiency, less dosage, excellent performance in cleaning and decontamination and removal of pesticides on the surface of fruits and vegetables, broad sterilization and antibacterial spectrum, and strong antibacterial ability; not only can wash away the dirt on fruits and vegetables , microorganisms and insect eggs, and will not change the nutritional content and taste of fruits and vegetables.

Description

technical field [0001] The invention relates to a cleaning agent and a preparation method thereof, in particular to a preparation method of a fruit and vegetable cleaning agent compounded with Schisandra chinensis extract and camellia oleifera cake extract. Background technique [0002] With the rapid development of my country's agriculture, the output of fruits and vegetables has increased year by year, the scope of use of pesticides has continued to expand, and the amount of pesticides has continued to increase. Fruits and vegetables are the most consumed food in people's daily life. The amount of residual pesticides and industrial pollutants adsorbed on fruits and vegetables is large, which has already posed a serious hazard to public health. According to statistics, the pesticides ingested by humans through food accounted for more than 90% of the total amount of pesticides ingested by humans, and the pesticides ingested through eating fruits and vegetables accounted for ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11D7/44C11D7/60C11D10/02
Inventor 于新陈新罗维英钟蓓邱苑新江秀娟
Owner ZHONGKAI UNIV OF AGRI & ENG
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