A light-weight equal-diameter microporous corundum composite sphere and its preparation method
An equal-diameter, micro-porous technology, applied in the field of micro-diameter and micro-porous corundum composite balls and its preparation, can solve the problems of light-weight materials that are difficult to meet the requirements, many slag diffusion channels, and complex slag erosion process, etc., and achieve thermal shock stability Good performance, strong erosion resistance and slag erosion resistance, low bulk density
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Embodiment 1
[0026] A light-weight equal-diameter microporous corundum composite sphere and a preparation method thereof. With 90~93wt% α-Al 2 o 3 Micropowder and 7-10wt% MgO micropowder as raw materials, plus dextrin accounting for 5-10wt% of the raw material, mixed with a planetary ball mill for 0.05-0.4 hours; then adding water accounting for 6-15wt% of the raw material, rotating granulation , that is, the prefabricated ball is obtained.
[0027] Alumina sol and ρ-Al 2 o 3 The fine powder is mixed into a slurry according to the mass ratio of (0.04~0.07):1, and then the slurry is evenly sprayed on the surface of the prefabricated ball, and the ratio of the thickness of the slurry sprayed on the surface of the prefabricated ball to the radius of the prefabricated ball is (0.08 ~0.12): 1; then dry at 110~160°C for 24~36 hours, and calcined at 1900~2000°C in an ultra-high temperature shaft kiln for 3~5 hours to obtain a lightweight equal-diameter microporous corundum composite ball . ...
Embodiment 2
[0030] A light-weight equal-diameter microporous corundum composite sphere and a preparation method thereof. With 90~93wt% γ-Al 2 o 3 Micropowder and 7-10wt% MgO micropowder are raw materials, plus starch accounting for 10-15wt% of the raw material, mixed with a planetary ball mill for 0.4-0.8 hours; then adding water accounting for 13-20wt% of the raw material, rotating granulation, Get the preformed ball.
[0031] Alumina sol and ρ-Al 2 o 3 The fine powder is mixed into a slurry according to the mass ratio of (0.07~0.1):1, and then the slurry is evenly sprayed on the surface of the prefabricated ball, and the ratio of the thickness of the slurry sprayed on the surface of the prefabricated ball to the radius of the prefabricated ball is (0.05 ~0.09): 1; then dry at 150~200°C for 12~24 hours, and calcined at 2000~2100°C for 2~4 hours in an ultra-high temperature shaft kiln to obtain a lightweight equal-diameter microporous corundum composite ball .
[0032] The light-wei...
Embodiment 3
[0034] A light-weight equal-diameter microporous corundum composite sphere and a preparation method thereof. With 92~95wt% α-Al 2 o 3 Micropowder and 5-8wt% MgO micropowder are raw materials, plus chitin accounting for 5-10wt% of the raw material, mixed with a planetary ball mill for 0.05-0.4 hours; then adding water accounting for 6-15wt% of the raw material, rotating granulation , that is, the prefabricated ball is obtained.
[0035] Alumina sol and ρ-Al 2 o 3The fine powder is mixed into a slurry according to the mass ratio of (0.04~0.07):1, and then the slurry is evenly sprayed on the surface of the prefabricated ball, and the ratio of the thickness of the slurry sprayed on the surface of the prefabricated ball to the radius of the prefabricated ball is (0.08 ~0.12): 1; then dry at 110~160°C for 24~36 hours, and calcined at 1900~2000°C in an ultra-high temperature shaft kiln for 3~5 hours to obtain a lightweight equal-diameter microporous corundum composite ball .
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